1,1-二甲酸乙酯环戊烷合成路线 (共 39 条)
反应条件
potassium carbonate; [bmim]Br in N,N-dimethyl-formamide T=20°C; 7 h;
参考文献
Muthusamy, Sengodagounder; Gnanaprakasam, Boopathy
Tetrahedron Letters, 2005 , vol. 46, # 4 p. 635 - 638
反应条件
1: With 1-n-butyl-3-methylimidazolium hexafluorophosphate in dichloromethane T=40°C; 1 h; Inert atmosphere; 2: With hydrogen in isopropyl alcohol T=20°C; P=760.051 Torr; 0.5 h; Inert atmosphere;
参考文献
Lee, Sujin; Shin, Ju Yeon; Lee, Sang-Gi
Chemistry - An Asian Journal, 2013 , vol. 8, # 9 p. 1990 - 1993
反应条件
hydrogen; dichlorobis(tricyclohexylphosphine)(benzylidene)rhodium in 1,2-dichloro-ethane T=70°C; P=760.051 Torr;
参考文献
Louie; Bielawski; Grubbs
Journal of the American Chemical Society, 2001 , vol. 123, # 45 p. 11312 - 11313
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene T=80°C; 2 h;
参考文献
Kim, Sunggak; Kee, In Seo; Lee, Sangphil
Journal of the American Chemical Society, 1991 , vol. 113, # 26 p. 9882 - 9883
反应条件
1: ethanol; pentane / 0 °C 2: 30 percent / n-Bu3SnH, AIBN / benzene / 4 h / 80 °C / var. N-aziridinyl imines View Scheme
参考文献
Kim, Sunggak; Kee, In Seo; Lee, Sangphil
Journal of the American Chemical Society, 1991 , vol. 113, # 26 p. 9882 - 9883
反应条件
1: ethanol; pentane / 0 °C 2: 75 percent / n-Bu3SnH, AIBN / benzene / 2 h / 80 °C View Scheme
参考文献
Kim, Sunggak; Kee, In Seo; Lee, Sangphil
Journal of the American Chemical Society, 1991 , vol. 113, # 26 p. 9882 - 9883
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene T=80°C; 4 h;
参考文献
Kim, Sunggak; Kee, In Seo; Lee, Sangphil
Journal of the American Chemical Society, 1991 , vol. 113, # 26 p. 9882 - 9883
参考文献
Bailey,W.J.; Daly,J.J.
Journal of Organic Chemistry, 1964 , vol. 29, p. 1249 - 1251
反应条件
ethanol; sodium ethanolate
参考文献
Tatarinova, V. I.; Vasil'ev, A. A.; Petrosyan, V. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 11 p. 2399 - 2401
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , # 11 p. 2646 - 2648
参考文献
Houk,J.; Whitesides,G.M.
Journal of the American Chemical Society, 1987 , vol. 109, p. 6825