反应条件
in tetrahydrofuran
under dry Ar at 0°C, stirred soln. of (C6H5)3SnLi treated dropwise with soln. of (C6H5)3SnCH2CH(CH2OSO2CH3)2, kept at 25°C for 18h, refluxed for 3 h; H2O added, evapd. (vac.), partitioned between H2O and CH2Cl2, org. phase dried, evapd. (vac.), chromd. (SiO2, hexanes/CHCl3), crystd. (hexanes/EtOAc); elem. anal.;
参考文献
Ducharme, Yves; Latour, Stephan; Wuest, James D.
Organometallics, 1984 , vol. 3, p. 208 - 211
