1: (2,4,6-trimethylphenyl)methyl alcohol With sodium chlorite; sodium dihydrogenphosphate; 1-MeAZADO(1+)*Cl(1-) in dichloromethane; water T=25°C; 4.5 h; 2: With 2-methyl-but-2-ene in dichloromethane; water 3: diazomethane With hydrogenchloride; sodium hydroxide Product distribution / selectivity; more than 3 stages;
参考文献
Nissan Chemical Industries, Ltd.
Patent: US2009/124806 A1, 2009 ;
Location in patent: Page/Page column 5-6 ;
1: With 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; 1,3-Diiodo-5,5-dimethyl-2,4-imidazolidinedione in dichloromethane T=20°C; 0.5 h; Inert atmosphere; 2: With ammonia; iodine in dichloromethane; water T=20°C; 2 h; Inert atmosphere;
