1-甲基-1H-咪唑-5-羰酰氯合成路线 （共 4 条）
反应条件
1 h; Heating; Yield given;
参考文献
Takahashi, Kazuyuki; Mitsuhashi, Keiryo
Bulletin of the Chemical Society of Japan, 1980 , vol. 53, # 2 p. 557 - 558
反应条件
oxalyl dichloride in dichloromethane
1 h; Heating / reflux;
参考文献
METHYLGENE, INC.
Patent: WO2006/10264 A1, 2006 ;
Location in patent: Page/Page column 118 ;
WO 2006/010264 A1
反应条件
1: 99 percent / Ac2O / 4 h / 100 °C / selectivity of decarboxylation; other acid anhydride; var. temp. reaction time and solvents
2: SOCl2 / 6 h / Heating
View Scheme
参考文献
Takahashi, Kazuyuki; Mitsuhashi, Keiryo
Bulletin of the Chemical Society of Japan, 1980 , vol. 53, # 2 p. 557 - 558
反应条件
pyridine in dichloromethane
T=40°C; 0.5 h;
参考文献
Fraley, Mark E.; Steen, Justin T.
Patent: US2009/182001 A1, 2009 ;
Location in patent: Page/Page column 18 ;
