4'-乙酰苯并-15-冠-5-醚合成路线 （共 13 条）
反应条件
1: 89 percent / bromine, sodium hydroxide / H2O / 0 - 10 °C 2: 99 percent / oxalyl chloride, pyridine / CH2Cl2 / 4 h / Ambient temperature 3: 80 percent / pyridine / 18 h / Ambient temperature View Scheme
参考文献
Haines, Alan H.; Hodgkisson, Ian; Smith, Christopher
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 311 - 318
反应条件
sodium hydroxide; bromine in water T=0 - 10°C;
参考文献
Haines, Alan H.; Hodgkisson, Ian; Smith, Christopher
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 311 - 318
反应条件
1: 91 percent / sodium borohydride / ethanol / 18 h / Ambient temperature
2: 90 percent / pyridinium tosylate / benzene / 18 h / Heating
View Scheme
参考文献
Talma, Auke G.; Vossen, Huib van; Sudhoelter, Ernst J. R.; Eerden, Johan van; Reinhoudt, David N.
Synthesis, 1986 , # 8 p. 680 - 683
