3,4-二氢-2H-苯并[C]氮杂卓-1,5-二酮合成路线 （共 34 条）
反应条件
aluminium trichloride in nitrobenzene
T=50°C; Curtius rearrangement; 5 h;
参考文献
Abdel-Fattah, A. A.; Nasar, S. A.; El-Shenawy, A. I.
Egyptian Journal of Chemistry, 2003 , vol. 46, # 1 p. 153 - 162
反应条件
potassium carbonate in water; acetone
T=15°C; Irradiation;
参考文献
Griesbeck, Axel G.; Henz, Andreas; Kramer, Wolfgang; Lex, Johann; Nerowski, Frank; Oelgemoeller, Michael; Peters, Karl; Peters, Eva-Maria
Helvetica Chimica Acta, 1997 , vol. 80, # 3 p. 912 - 933
反应条件
in methanol
8 h; Photolysis;
参考文献
Ung Chan Yoon; Sun Wha Oh; Jae Ho Lee; Jong Hoon Park; Kyung Tae Kang; Mariano
Journal of Organic Chemistry, 2001 , vol. 66, # 3 p. 939 - 943
反应条件
in methanol
8 h; Photolysis;
参考文献
Ung Chan Yoon; Sun Wha Oh; Jae Ho Lee; Jong Hoon Park; Kyung Tae Kang; Mariano
Journal of Organic Chemistry, 2001 , vol. 66, # 3 p. 939 - 943
反应条件
potassium carbonate in water; acetone
T=20°C; 12 h; Irradiation; Title compound not separated from byproducts;
参考文献
Griesbeck, Axel G.; Henz, Andreas; Peters, Karl; Peters, Eva-Maria; Schnering, Hans Georg von
Angewandte Chemie, 1995 , vol. 107, # 4 p. 498 - 500
反应条件
1: 92 percent / K2CO3 / dimethylsulfoxide / 24 h / 30 - 60 °C
2: 5 percent / acetone / 8 h / 10 - 20 °C / Irradiation
View Scheme
参考文献
Sato, Yasuhiko; Nakai, Hideo; Wada, Masao; Mizoguchi, Tomishige; Hatanaka, Yasumaru; et al.
Liebigs Annalen der Chemie, 1985 , # 6 p. 1099 - 1118
反应条件
in acetone
T=10 - 20°C; 3 h; Irradiation;
参考文献
Sato, Yasuhiko; Nakai, Hideo; Wada, Masao; Mizoguchi, Tomishige; Hatanaka, Yasumaru; et al.
Liebigs Annalen der Chemie, 1985 , # 6 p. 1099 - 1118
反应条件
in acetone
T=10 - 20°C; 2 h; Irradiation;
参考文献
Sato, Yasuhiko; Nakai, Hideo; Wada, Masao; Mizoguchi, Tomishige; Hatanaka, Yasumaru; et al.
Liebigs Annalen der Chemie, 1985 , # 6 p. 1099 - 1118
反应条件
potassium carbonate in acetone
Irradiation;
参考文献
Griesbeck, Axel G.
Chimia, 1998 , vol. 52, # 6 p. 272 - 283
反应条件
in methanol
8 h; Photolysis;
参考文献
Ung Chan Yoon; Sun Wha Oh; Jae Ho Lee; Jong Hoon Park; Kyung Tae Kang; Mariano
Journal of Organic Chemistry, 2001 , vol. 66, # 3 p. 939 - 943
