N,N-二异丙基丁烷-1-胺合成路线 (共 3 条)
反应条件
hydrogen; 5 Pd(II)/C(eggshell)
T=120°C; P=37503.8 Torr; AutoclaveInert atmosphereIndustry scale; Product distribution / selectivity;
参考文献
BASF SE
Patent: US2010/267948 A1, 2010 ;
Location in patent: Page/Page column 6-7 ;
反应条件
oxygen in tetrahydrofuran
1.) -40 deg C, 15 min, 2.) -78 deg C, 20 min;
参考文献
Alberti, Angelo; Cane, Francesco; Dembech, Pasquale; Lazzari, Dario; Ricci, Alfredo; Seconi, Giancarlo
Journal of Organic Chemistry, 1996 , vol. 61, # 5 p. 1677 - 1681
反应条件
oxygen; zinc(II) chloride
Yield given. Multistep reaction;
参考文献
Cane; Brancaleoni; Dembech; Ricci; Seconi
Synthesis, 1997 , # 5 p. 545 - 548