1.1: sodium perchlorate / diethyl ether / 0.5 h / 0 °C / |Inert atmosphere 2.1: diethyl ether / 2 h / 0 °C / |Inert atmosphere 2.2: 24 h / 80 °C / |Inert atmosphere View Scheme

sodium perchlorate in diethyl ether T=0°C; 0.5 h; Inert atmosphere;