5-氨基-3,4-二氢-2H-1-萘酮合成路线 （共 13 条）
反应条件
palladium on activated carbon in diethylene glycol dimethyl ether
T=130°C; 18 h;
参考文献
Mitsui Chemicals, Inc.
Patent: US2004/143137 A1, 2004 ;
Location in patent: Page 4 ;
反应条件
ammonium chloride in methanol; water
参考文献
Schelhaas, Michael; Joschek, Katrin; Jautelat, Manfred; Zechlin, Joachim; Wastian, Dietmar
Patent: US2002/103401 A1, 2002 ;
反应条件
aluminum tri-bromide; cyclohexane
T=110°C; 40 h;
参考文献
Koltunov, Konstantin Yu; Surya Prakash; Rasul, Golam; Olah, George A
Tetrahedron, 2002 , vol. 58, # 27 p. 5423 - 5426
参考文献
Schelhaas, Michael; Joschek, Katrin; Jautelat, Manfred; Zechlin, Joachim; Wastian, Dietmar
Patent: US2002/103401 A1, 2002 ;
反应条件
1: 70 percent / K2CO3 / dimethylformamide / 1 h / Ambient temperature
2: 100 percent / 0.33 h / 170 °C
3: 98 percent / NaOH / methanol / 1 h / Heating
4: Raney nickel / ethanol / 2 h / Heating
View Scheme
参考文献
Itoh; Miyake; Tada; Hirata; Oka
Chemical and Pharmaceutical Bulletin, 1984 , vol. 32, # 1 p. 130 - 151
反应条件
1: 98 percent / NaOH / methanol / 1 h / Heating
2: Raney nickel / ethanol / 2 h / Heating
View Scheme
参考文献
Itoh; Miyake; Tada; Hirata; Oka
Chemical and Pharmaceutical Bulletin, 1984 , vol. 32, # 1 p. 130 - 151
反应条件
1: 100 percent / 0.33 h / 170 °C
2: 98 percent / NaOH / methanol / 1 h / Heating
3: Raney nickel / ethanol / 2 h / Heating
View Scheme
参考文献
Itoh; Miyake; Tada; Hirata; Oka
Chemical and Pharmaceutical Bulletin, 1984 , vol. 32, # 1 p. 130 - 151
参考文献
Schelhaas, Michael; Joschek, Katrin; Jautelat, Manfred; Zechlin, Joachim; Wastian, Dietmar
Patent: US2002/103401 A1, 2002 ;
反应条件
hydrogenchloride; iron(II) sulfate; tin(ll) chloride
参考文献
Nakamura
Yakugaku Zasshi, 1941 , vol. 61, p. 292,294; dtsch. Ref. S. 108
Chem.Abstr., 1950 , p. 9389
反应条件
nickel in ethanol
2 h; Heating; Yield given;
参考文献
Itoh; Miyake; Tada; Hirata; Oka
Chemical and Pharmaceutical Bulletin, 1984 , vol. 32, # 1 p. 130 - 151
