反应条件
in diethyl ether
InBr3 is dissolved in Et2O, at 0°C is added LiCH(SiMe3)2 in Et2O, the soln. is heated under reflux for 2.5 h, (under exclusion of light).; distn. of solvent under vac., to the residue is added pentane, filtn., drying of filtrate, sublimation of product (1E-4 Torr, oil bath temp. of 100°C);
参考文献
Uhl, Werner; Layh, Marcus; Hiller, Wolfgang
Journal of Organometallic Chemistry, 1989 , vol. 368, p. 139 - 154
