5,6-二甲基-1H-苯并三唑水合物合成路线 (共 11 条)
参考文献
Valizadeh, Hassan; Gholipour, Hamid; Mahmoodian, Manzar
Synthetic Communications, 2013 , vol. 43, # 20 p. 2801 - 2808
反应条件
1: conc. HCl, NaNO2 / H2O / 1 h / Ambient temperature 2: conc. HCl / 2 h / Heating View Scheme
参考文献
Risitano, Francesco; Grassi, Giovanni; Foti, Francesco; Caruso, Francesco
Journal of Chemical Research, Miniprint, 1983 , # 2 p. 352 - 357
反应条件
hydrogenchloride 2 h; Heating; Yield given;
参考文献
Risitano, Francesco; Grassi, Giovanni; Foti, Francesco; Caruso, Francesco
Journal of Chemical Research, Miniprint, 1983 , # 2 p. 352 - 357
反应条件
in benzene-d6 Equilibrium constant;
参考文献
Katritzky, Alan R.; Perumal, Subbu; Savage, G. Paul
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1990 , # 6 p. 921 - 924
反应条件
in benzene-d6 Equilibrium constant;
参考文献
Katritzky, Alan R.; Perumal, Subbu; Savage, G. Paul
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1990 , # 6 p. 921 - 924
反应条件
triethylamine in dichloromethane
Acylation;
参考文献
Katritzky; Huang; Voronkov; Steel
Journal of Organic Chemistry, 2000 , vol. 65, # 23 p. 8069 - 8073
参考文献
Benson et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 4917,4919
反应条件
1: 94 percent / 0.5 h / 150 - 200 °C
2: 78 percent / H4P2O7 / 0.07 h / Irradiation
View Scheme
参考文献
Molina; Vaquero; Garcia-Navio; Alvarez-Builla; De Pascual-Teresa; Gago; Rodrigo; Ballesteros
Journal of Organic Chemistry, 1996 , vol. 61, # 16 p. 5587 - 5599
反应条件
dihydrogenpyrophosphate
multistep reaction under microwave irradiation, other substrates; Product distribution;
参考文献
Molina, Andres; Vaquero, Juan J.; Garcia-Navio, Jose L.; Alvarez-Builla, Julio
Tetrahedron Letters, 1993 , vol. 34, # 16 p. 2673 - 2676
反应条件
1: 92 percent / 0.5 h / 150 - 200 °C
2: 85 percent / H4P2O7 / 150 °C
View Scheme
参考文献
Molina; Vaquero; Garcia-Navio; Alvarez-Builla; De Pascual-Teresa; Gago; Rodrigo; Ballesteros
Journal of Organic Chemistry, 1996 , vol. 61, # 16 p. 5587 - 5599