2-氯-4''-甲氧基苯偶酰合成路线 （共 11 条）
反应条件
silica gel; iron nitrate (III) in 1,2-dichloro-ethane
3 h; Heating;
参考文献
Paul, Aniruddha M.; Khandekar, Amit C.; Shenoy
Synthetic Communications, 2003 , vol. 33, # 15 p. 2581 - 2584
反应条件
formaldehyd; trifluoroacetic acid in chloroform
72 h; Ambient temperature;
参考文献
Yamamori, Teruo; Adachi, Ikuo
Tetrahedron Letters, 1980 , vol. 21, p. 1747 - 1750
反应条件
selenium(IV) oxide in dimethyl sulfoxide
0.025 h; microwave irradiation;
参考文献
Shirude; Patel; Giridhar; Yadav
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2006 , vol. 45, # 4 p. 1080 - 1085
反应条件
1: potassium cyanide; aqueous ethanol
2: ethanol; Fehling solution
View Scheme
参考文献
Buck; Ide
Journal of the American Chemical Society, 1930 , vol. 52, p. 4107,4109
Journal of the American Chemical Society, 1931 , vol. 53, p. 1536,1540
反应条件
1: potassium cyanide; aqueous ethanol
2: ethanol; Fehling solution
View Scheme
参考文献
Buck; Ide
Journal of the American Chemical Society, 1930 , vol. 52, p. 4107,4109
Journal of the American Chemical Society, 1931 , vol. 53, p. 1536,1540
反应条件
1: 1.) n-BuLi / 1.) TMEDA, -78 deg C, 2.) THF, -78 deg C, overnight
2: 72.8 percent / CF3COOH, 35 percent aq CH2O / CHCl3 / 72 h / Ambient temperature
View Scheme
参考文献
Yamamori, Teruo; Adachi, Ikuo
Tetrahedron Letters, 1980 , vol. 21, p. 1747 - 1750
反应条件
1: 1.) n-BuLi / 1.) TMEDA, -78 deg C, 2.) THF, -78 deg C, overnight
2: 72.8 percent / CF3COOH, 35 percent aq CH2O / CHCl3 / 72 h / Ambient temperature
View Scheme
参考文献
Yamamori, Teruo; Adachi, Ikuo
Tetrahedron Letters, 1980 , vol. 21, p. 1747 - 1750
反应条件
1: n-BuLi / tetrahydrofuran
2: 1.) n-BuLi / 1.) TMEDA, -78 deg C, 2.) THF, -78 deg C, overnight
3: 72.8 percent / CF3COOH, 35 percent aq CH2O / CHCl3 / 72 h / Ambient temperature
View Scheme
参考文献
Yamamori, Teruo; Adachi, Ikuo
Tetrahedron Letters, 1980 , vol. 21, p. 1747 - 1750
反应条件
1: PCl3
2: 52 percent / anhydrous AlCl3
3: 82 percent / selenium dioxide / dimethylsulfoxide / 0.03 h / microwave irradiation
View Scheme
参考文献
Shirude; Patel; Giridhar; Yadav
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2006 , vol. 45, # 4 p. 1080 - 1085
反应条件
1: 52 percent / anhydrous AlCl3
2: 82 percent / selenium dioxide / dimethylsulfoxide / 0.03 h / microwave irradiation
View Scheme
参考文献
Shirude; Patel; Giridhar; Yadav
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2006 , vol. 45, # 4 p. 1080 - 1085
