氯化-1-(2,4-二硝基苯基)吡啶嗡盐合成路线 (共 58 条)
反应条件
ethanol 1.5 h; Heating;
参考文献
Steinhardt, Sarah E.; Silverston, Joel S.; Vanderwal, Christopher D.
Journal of the American Chemical Society, 2008 , vol. 130, # 24 p. 7560 - 7561
反应条件
in methanol T=20°C; Zincke reaction; 20 h; Inert atmosphereReflux;
参考文献
Robertson, Linsey; Hartley, Richard C.
Tetrahedron, 2009 , vol. 65, # 27 p. 5284 - 5292
反应条件
in ethanol 12 h; Heating;
参考文献
Yamaguchi, Isao; Gobara, Yoshiaki; Sato, Moriyuki
Organic Letters, 2006 , vol. 8, # 19 p. 4279 - 4281
反应条件
in ethanol 12 h; Heating; Title compound not separated from byproducts;
参考文献
Yamaguchi, Isao; Gobara, Yoshiaki; Sato, Moriyuki
Organic Letters, 2006 , vol. 8, # 19 p. 4279 - 4281
反应条件
in ethanol 12 h; Heating;
参考文献
Yamaguchi, Isao; Gobara, Yoshiaki; Sato, Moriyuki
Organic Letters, 2006 , vol. 8, # 19 p. 4279 - 4281
反应条件
aniline in N,N-dimethyl-formamide T=0°C; 1 h;
参考文献
Esteve, Marta E.; Gaozza, Carlos H.
Journal of Heterocyclic Chemistry, 1981 , vol. 18, p. 1061 - 1063
反应条件
in methanol Zincke reaction; 18 h; Inert atmosphereReflux;
参考文献
Robertson, Linsey; Hartley, Richard C.
Tetrahedron, 2009 , vol. 65, # 27 p. 5284 - 5292
反应条件
1: N-tert-butyl-α-(2-hexyloxy-5-nitrophenyl)nitrone With 10 Pd(OH)2/C; hydrogen in ethyl acetate T=20°C; 0.5 h; 2: N-(2,4-dinitrophenyl)-pyridinium chloride in methanol Zincke reaction; 18 h; Reflux;
参考文献
Robertson, Linsey; Hartley, Richard C.
Tetrahedron, 2009 , vol. 65, # 27 p. 5284 - 5292
反应条件
in ethanol 12 h; Heating;
参考文献
Yamaguchi, Isao; Gobara, Yoshiaki; Sato, Moriyuki
Organic Letters, 2006 , vol. 8, # 19 p. 4279 - 4281
反应条件
in methanol Zincke reaction; 48 h; Inert atmosphereReflux;
参考文献
Robertson, Linsey; Hartley, Richard C.
Tetrahedron, 2009 , vol. 65, # 27 p. 5284 - 5292