三甲基(对甲苯乙炔)硅烷合成路线 （共 36 条）
反应条件
n-butyllithium
Yield given. Multistep reaction;
参考文献
Paquette, Leo A.; Fristad, William E.; Dime, David S.; Bailey, Thomas R.
Journal of Organic Chemistry, 1980 , vol. 45, # 15 p. 3017 - 3028
反应条件
1: hexadeuterioacetone / -80 °C
2: hexadeuterioacetone
View Scheme
参考文献
Sharma, Manab; Ariafard, Alireza; Canty, Allan J.; Yates, Brian F.; Gardiner, Michael G.; Jones, Roderick C.
Dalton Transactions, 2012 , vol. 41, # 38 p. 11820 - 11828
反应条件
in hexadeuterioacetone
参考文献
Sharma, Manab; Ariafard, Alireza; Canty, Allan J.; Yates, Brian F.; Gardiner, Michael G.; Jones, Roderick C.
Dalton Transactions, 2012 , vol. 41, # 38 p. 11820 - 11828
反应条件
in hexadeuterioacetone
参考文献
Sharma, Manab; Ariafard, Alireza; Canty, Allan J.; Yates, Brian F.; Gardiner, Michael G.; Jones, Roderick C.
Dalton Transactions, 2012 , vol. 41, # 38 p. 11820 - 11828
反应条件
in hexadeuterioacetone
KineticsActivation energy; TemperatureSolventConcentrationReagent/catalyst;
参考文献
Sharma, Manab; Ariafard, Alireza; Canty, Allan J.; Yates, Brian F.; Gardiner, Michael G.; Jones, Roderick C.
Dalton Transactions, 2012 , vol. 41, # 38 p. 11820 - 11828
反应条件
1: With cesium fluoride in dimethyl sulfoxide
T=20°C; 3 h; Schlenk technique;
2: With hydrogenchloride in water
T=0°C; pH=> 1;
参考文献
Yonemoto-Kobayashi, Misato; Inamoto, Kiyofumi; Tanaka, Yoshiyuki; Kondo, Yoshinori
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 23 p. 3773 - 3775
反应条件
copper(l) iodide; palladium; triphenylphosphine; aluminum oxide; potassium fluoride
Sonogashira coupling reaction; 0.0416667 h; microwave irradiation;
参考文献
Kabalka, George W.; Wang, Lei; Pagni, Richard M.
Tetrahedron, 2001 , vol. 57, # 38 p. 8017 - 8028
反应条件
1: 96 percent / KOH
View Scheme
参考文献
Al-Hassan, Mohammed I.
Journal of Organometallic Chemistry, 1990 , vol. 395, # 2 p. 227 - 229
反应条件
silver nitrate in tetrahydrofuran; water
T=20°C; 24 h; Inert atmosphere;
参考文献
Deng, Gui Sheng; Sun, Teng Fei
Chinese Chemical Letters, 2012 , vol. 23, # 10 p. 1115 - 1118,4
反应条件
potassium fluoride in dimethyl sulfoxide
T=20°C; 16 h;
参考文献
Klukas, Fabian; Grunwald, Alexander; Menschel, Franziska; Mueller, Thomas J. J.
Beilstein Journal of Organic Chemistry, 2014 , vol. 10, p. 672 - 679
