1-苯基-2-丙炔-1-醇合成路线 （共 176 条）
反应条件
1: acetone; CrO3; aqueous H2SO4 / 5 °C 2: methanol View Scheme
参考文献
Bowden; Jones
Journal of the Chemical Society, 1946 , p. 52
反应条件
1: With hydrogen iodide in toluene T=20°C; 0.0833333 h; 2: With oxygen in toluene T=50°C; 4 h; Further stages.;
参考文献
Chen, Shufeng; Wang, Jianbo
Journal of Organic Chemistry, 2007 , vol. 72, # 13 p. 4993 - 4996
反应条件
NH4BF4; [(Cp*)RuCl(SMe)]2 in 1,2-dichloro-ethane T=60°C; 1 h;
参考文献
Nishibayashi, Yoshiaki; Milton, Marilyn Daisy; Inada, Youichi; Yoshikawa, Masato; Wakiji, Issei; Hidai, Masanobu; Uemura, Sakae
Chemistry - A European Journal, 2005 , vol. 11, # 5 p. 1433 - 1451
反应条件
sodium hydroxide; tetrabutyl-ammonium chloride in hexane Ambient temperature;
参考文献
Trost, Barry M.; Edstrom, Eric D.; Carter-Petillo, Mary Beth
Journal of Organic Chemistry, 1989 , vol. 54, # 19 p. 4489 - 4490
反应条件
NH4BF4; [(Cp*)RuCl(SMe)]2 in 1,2-dichloro-ethane T=20°C; 2 h;
参考文献
Nishibayashi, Yoshiaki; Milton, Marilyn Daisy; Inada, Youichi; Yoshikawa, Masato; Wakiji, Issei; Hidai, Masanobu; Uemura, Sakae
Chemistry - A European Journal, 2005 , vol. 11, # 5 p. 1433 - 1451
反应条件
sulfuric acid; sodium sulfate T=-20 - 20°C; Substitution; Ritter reaction; 48 h;
参考文献
Messina; Botta; Corelli; Schneider; Fazio
Journal of Organic Chemistry, 1999 , vol. 64, # 10 p. 3767 - 3769
反应条件
sulfuric acid; sodium sulfate 48 h; Ambient temperature;
参考文献
Nilsson, Bjoern M.; Hacksell, Uli
Journal of Heterocyclic Chemistry, 1989 , vol. 26, p. 269 - 275
反应条件
sulfuric acid; sodium sulfate T=-20 - 20°C; Ritter reaction;
参考文献
Nilsson, Bjoern M.; Hacksell, Uli
Journal of Heterocyclic Chemistry, 1989 , vol. 26, p. 269 - 275
反应条件
1: triethylamine / diethyl ether / -78 °C
2: sodium amide / diethyl ether; liquid ammonia / 5 h / -40 °C
3: pyridine / diethyl ether / 3 h
4: 93 percent / sodium hydride / tetrahydrofuran / 0.2 h / 20 °C / other temperature, time, base
View Scheme
参考文献
Nilsson, Bjoern M.; Hacksell, Uli
Journal of Heterocyclic Chemistry, 1989 , vol. 26, p. 269 - 275
反应条件
gold(III) chloride; NH4BF4; [(η5-C5Me5)RuCl(μ2-SMe)2Ru(η5-C5Me5)Cl]
36 h; Heating;
参考文献
Nishibayashi, Yoshiaki; Yoshikawa, Masato; Inada, Youichi; Milton, Marilyn Daisy; Hidai, Masanobu; Uemura, Sakae
Angewandte Chemie - International Edition, 2003 , vol. 42, # 23 p. 2681 - 2684
