1-苯基-2-丙炔-1-醇合成路线 （共 176 条）
反应条件
in tetrahydrofuran; toluene; xylene 1 h; Ambient temperature;
参考文献
Joung, Meyoung Ju; Ahn, Jin Hee; Yoon, Nung Min
Journal of Organic Chemistry, 1996 , vol. 61, # 13 p. 4472 - 4475
反应条件
magnesium in tetrahydrofuran; diethyl ether
参考文献
Gharibyan; Makaryan; Hovhannisyan; Kinoyan; Chobanyan
Russian Journal of General Chemistry, 2014 , vol. 84, # 3 p. 457 - 464
Zh. Obshch. Khim., 2014 , vol. 84, # 3 p. 399 - 406,8
反应条件
in tetrahydrofuran T=0 - 20°C; addition of monolithium acetylide to various electrophiles in THF at 0 deg C; reversible disproportionation of monolithium acetylide into dilithium carbide and acetylene in THF at 0 deg C; Product distribution;
参考文献
Mortier, Jacques; Vaultier, Michel; Carreaux, Francois; Douin, Jean-Marc
Journal of Organic Chemistry, 1998 , vol. 63, # 10 p. 3515 - 3516
反应条件
potassium fluoride; C46H34I4O6 in 1,4-dioxane T=20°C; 144 h; optical yield given as percent eeenantioselective reaction;
参考文献
Yan, Hailong; Jang, Hyeong Bin; Lee, Ji-Woong; Kim, Hong Ki; Lee, Soon Won; Yang, Jung Woon; Song, Choong Eui
Angewandte Chemie - International Edition, 2010 , vol. 49, # 47 p. 8915 - 8917
反应条件
(2S,2'S)-2-hydroxymethyl-1-lt;(1-methylpyrrolidine-2-yl)methylgt;pyrrolidine investigation of the asymmetric addition of lithium trimethylsilylacetylides in presence (2S,2'S)-2-hydroxymethyl-1-<(1-methylpyrrolidine-2-yl)methyl>pyrrolidine; Product distributionMechanism;
参考文献
Mukaiyama, Teruaki
Tetrahedron, 1981 , vol. 37, # 23 p. 4111 - 4119
参考文献
Cymerman; Wilks
Journal of the Chemical Society, 1950 , p. 1208
反应条件
diethyl ether nachfolgend Einw. von Benzaldehyd;
参考文献
Lespieau
Bulletin de la Societe Chimique de France, 1926 , vol. <4>39, p. 994
Bulletin de la Societe Chimique de France, 1928 , vol. <4>43, p. 657
反应条件
1.) THF, hexane, -78 deg C, 20 min, 2.) from -78 deg C to RT, 2 h,; Yield given. Multistep reaction;
参考文献
Henderson, Mark, A.; Heathcock, Clayton, H.
Journal of Organic Chemistry, 1988 , vol. 53, # 20 p. 4736 - 4745
参考文献
Clapperton; MacGregor
Journal of the American Chemical Society, 1949 , vol. 71, p. 3234
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Jones; McCombie
Journal of the Chemical Society, 1942 , p. 733
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Campbell; Campbell; Eby
Journal of the American Chemical Society, 1938 , vol. 60, p. 2882
反应条件
in diethyl ether; pentane T=-75°C; 1 h; var. temp.; thermal stability of the lithio-deriv.; Product distribution;
参考文献
Baudrillard, Vincent; Ple, Gerard; Davoust, Daniel; Duhamel, Lucette
Journal of Chemical Research, Miniprint, 1997 , # 12 p. 2820 - 2831
