1-苯基-2-丙炔-1-醇合成路线 (共 176 条)
反应条件
water; ruthenium hydroxyapatite T=80°C; anti-Markovnikov hydration; 24 h; Product distribution; Further Variations:Catalysts;
参考文献
European Journal of Inorganic Chemistry, , # 4 p. 810 - 817
反应条件
water; mercuric sulphate
参考文献
Faworskii <Favorsky>; Temnikowa
Zhurnal Obshchei Khimii, 1934 , vol. 4, p. 745,753
Bulletin de la Societe Chimique de France, 1935 , vol. <5> 2, p. 253,262
反应条件
zuletzt unter Erwaermen auf dem Dampfbad;
参考文献
Faworskii <Favorsky>; Temnikowa
Zhurnal Obshchei Khimii, 1934 , vol. 4, p. 745,753
Bulletin de la Societe Chimique de France, 1935 , vol. <5> 2, p. 253,262
反应条件
1: 86 percent / Pd(PPh3)2Cl2; CuI; Et3N / dimethylformamide / 24 h / 20 °C 2: 73 percent / p-toluenesulfonic acid / benzene / 24 h / 20 °C 3: 68 percent / p-toluenesulfonic acid / benzene / 8 h / Heating View Scheme
参考文献
De, Mahuya; Majumdar, Dyuti P.; Kundu, Nitya G.
Journal of the Indian Chemical Society, 1999 , vol. 76, # 11-12 p. 665 - 674
反应条件
1: HgSO4; aqueous methanol.H2SO4 2: platinum; methanol / 36775.4 Torr / Hydrogenation View Scheme
参考文献
Murahashi; Hagihara
Memoirs of the Institute of Scientific and Industrial Research, Osaka University, 1948 , vol. 6, p. 96,98
参考文献
Raj, C. Paul; Dhas, N. Arul; Cherkinski; Gedanken; Braverman
Tetrahedron Letters, 1998 , vol. 39, # 30 p. 5413 - 5416
反应条件
triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide in tetrahydrofuran Sonogashira coupling-isomerization reaction; 8 h; Heating;
参考文献
Braun, Roland U.; Ansorge, Markus; Mueller, Thomas J. J.
Chemistry - A European Journal, 2006 , vol. 12, # 35 p. 9081 - 9094
反应条件
mercury(II) diacetate in chloroform 7 h; Heating;
参考文献
Barluenga, Jose; Aznar, Fernando; Liz, Ramon; Cabal, Maria-Paz
Synthesis, 1985 , # 3 p. 313 - 314
反应条件
pyridine in diethyl ether; dichloromethane T=0 - 20°C;
参考文献
He, Guangke; Fu, Chunling; Ma, Shengming
Tetrahedron, 2009 , vol. 65, # 38 p. 8035 - 8042
反应条件
1: 1.) (PPh3)2PdCl2, CuI, Et3N / 1.) RT, 0.5 h, 2.) RT, 48 h 2: 86 percent / CrO3, H2SO4 / acetone / 0.75 h / Ambient temperature View Scheme
参考文献
Kundu, Nitya G.; Pal, Manojit; Chowdhury, Chinmay
Journal of Chemical Research, Miniprint, 1995 , # 1 p. 101 - 123