1-苯基-2-丙炔-1-醇合成路线 （共 176 条）
反应条件
1: 89 percent / LAH / diethyl ether / 18 h / Ambient temperature 2: 80 percent / Jones' reagent / acetone / 0.5 h / 0 °C View Scheme
参考文献
Kundu; Dasgupta; Chaudhuri; Mahanty; Spears; Shahinian
European Journal of Medicinal Chemistry, 1993 , vol. 28, # 6 p. 473 - 479
反应条件
toluene-4-sulfonic acid; [NBu4][ReO4] in dichloromethane 2 h; Ambient temperature;
参考文献
Narasaka, Koichi; Kusama, Hiroyuki; Hayashi, Yujiro
Chemistry Letters, 1991 , # 8 p. 1413 - 1416
Title/Abstract Full Text Show Details
Narasaka; Kusama; Hayashi
Tetrahedron, 1992 , vol. 48, # 11 p. 2059 - 2068
反应条件
pyridinium p-toluenesulfonate in acetonitrile T=80°C; 24 h;
参考文献
Sanz, Roberto; Martinez, Alberto; Alvarez-Gutierrez, Julia M.; Rodriguez, Felix
European Journal of Organic Chemistry, 2006 , # 6 p. 1383 - 1386
反应条件
pyridinium p-toluenesulfonate in acetonitrile T=80°C; 24 h;
参考文献
Sanz, Roberto; Martinez, Alberto; Alvarez-Gutierrez, Julia M.; Rodriguez, Felix
European Journal of Organic Chemistry, 2006 , # 6 p. 1383 - 1386
反应条件
sulfuric acid; sodium sulfate 48 h; Ambient temperature;
参考文献
Journal of Heterocyclic Chemistry, , vol. 26, p. 269 - 275
反应条件
[Rh(CO)2I]2; lithium iodide in methanol T=90°C; P=3750.38 Torr; 18 h; AutoclaveInert atmosphere;
参考文献
Dheur, Julien; Sauthier, Mathieu; Castanet, Yves; Mortreuxa, Andre
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 2-3 p. 557 - 561
反应条件
1.1: 54 percent / NaH / tetrahydrofuran / 0.5 h / 20 °C 2.1: nBuLi / tetrahydrofuran; hexane / 0.5 h / 0 °C 2.2: 93 percent / tetrahydrofuran; hexane / 0 - 20 °C 3.1: 59 percent / [Rh(rac-BINAP)]BF4 / 1,2-dichloro-ethane / 1 h / 80 °C View Scheme
参考文献
Tanaka, Ken; Shoji, Takeaki; Hirano, Masao
European Journal of Organic Chemistry, 2007 , # 16 p. 2687 - 2699
反应条件
hydrogen; TMSB; palladium in ethanol T=20°C; P=760 Torr; 20 h;
参考文献
Belotti, Damien; Cantagrel, Guillaume; Combellas, Catherine; Cossy, Janine; Kanoufi, Frederic; Nunige, Sandra
New Journal of Chemistry, 2005 , vol. 29, # 6 p. 761 - 764
反应条件
trifluoroacetic acid; [Ru(η3-2-C3H4Me)(CO)(1,1'-(Ph2P)2-ferrocene)][SbF6] in tetrahydrofuran Meyer-Schuster rearrangement; 3.5 h; Heating;
参考文献
Advanced Synthesis and Catalysis, , vol. 348, # 1-2 p. 101 - 110
反应条件
[(p-cumene)Ru(OTf)(CO)(PCy3)][OTf] in acetone T=60°C; 3 h;
参考文献
Advanced Synthesis and Catalysis, , vol. 349, # 6 p. 933 - 942
