1-苯基-2-丙炔-1-醇合成路线 （共 176 条）
反应条件
polyvanadioorganosiloxane (4percent vanadium) in xylene T=145 - 148°C;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 19, # 4 p. 715 - 721
Zhurnal Organicheskoi Khimii, , vol. 19, # 4 p. 808 - 815
反应条件
water; ruthenium hydroxyapatite T=80°C; anti-Markovnikov hydration; 24 h; Product distribution; Further Variations:Catalysts;
参考文献
European Journal of Inorganic Chemistry, , # 4 p. 810 - 817
反应条件
unter Durchleiten von Wasserdampf;
参考文献
Journal of the American Chemical Society, , vol. 70, p. 3953
反应条件
water; mercuric sulphate
参考文献
Zhurnal Obshchei Khimii, , vol. 4, p. 745,753
Bulletin de la Societe Chimique de France, , vol. <5> 2, p. 253,262
反应条件
zuletzt unter Erwaermen auf dem Dampfbad;
参考文献
Zhurnal Obshchei Khimii, , vol. 4, p. 745,753
Bulletin de la Societe Chimique de France, , vol. <5> 2, p. 253,262
反应条件
1.1: 54 percent / NaH / tetrahydrofuran / 0.5 h / 20 °C 2.1: nBuLi / tetrahydrofuran; hexane / 0.5 h / 0 °C 2.2: 93 percent / tetrahydrofuran; hexane / 0 - 20 °C 3.1: 63 percent / LiAlH4 / tetrahydrofuran; diethyl ether / 0.5 h / 0 °C 4.1: 89 percent / [Rh(rac-BINAP)]BF4 / 1,2-dichloro-ethane / 1 h / 80 °C View Scheme
参考文献
Tanaka, Ken; Shoji, Takeaki; Hirano, Masao
European Journal of Organic Chemistry, 2007 , # 16 p. 2687 - 2699
反应条件
copper(l) iodide; tetra(n-butyl)ammonium hydroxide; bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran; water T=80°C; Sonogashira coupling; 24 h;
参考文献
Cho, Chan Sik
Journal of Organometallic Chemistry, 2005 , vol. 690, # 17 p. 4094 - 4097
反应条件
copper(l) iodide; tetrabutyl ammonium fluoride; bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran T=80°C; 40 h;
参考文献
Journal of Organometallic Chemistry, , vol. 690, # 17 p. 4094 - 4097
反应条件
1: 68 percent / Et3N / (Ph3P)2PdCl2 / 24 h / 20 °C 2: 87 percent / sodium ethoxide / ethanol / 5 h / Heating View Scheme
参考文献
Kundu, Nitya G.; Mahanty, Jyan S.; Das, Palas; Das, Biswajit
Tetrahedron Letters, 1993 , vol. 34, # 10 p. 1625 - 1628
反应条件
potassium tert-butylate in toluene T=100°C; 4 h; Inert atmosphere;
参考文献
Wang, Xu; Pan, Ying-Ming; Huang, Xiao-Chao; Mao, Zhong-Yuan; Wang, Heng-Shan
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 13 p. 2028 - 2032
