2H-二苯并呋喃-3-羰酰氯合成路线 (共 16 条)
反应条件
thionyl chloride in benzene
3 h; Heating;
参考文献
Gupta, R. C.; Pratap, Ram; Prasad, C. R.; Anand, Nitya
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 4 p. 344 - 347
反应条件
1: K2CO3 / dimethylformamide / 4 h / 100 - 135 °C
2: 46 percent / trifluoroacetic acid / Ambient temperature
3: oxalyl chloride / dimethylformamide; CH2Cl2 / 2 h
View Scheme
参考文献
Satoh; Stanton; Hutchison; Libby; Kowalski; Lee; White; Kimble
Journal of Medicinal Chemistry, 1993 , vol. 36, # 23 p. 3580 - 3594
反应条件
1: 46 percent / trifluoroacetic acid / Ambient temperature
2: oxalyl chloride / dimethylformamide; CH2Cl2 / 2 h
View Scheme
参考文献
Satoh; Stanton; Hutchison; Libby; Kowalski; Lee; White; Kimble
Journal of Medicinal Chemistry, 1993 , vol. 36, # 23 p. 3580 - 3594
反应条件
1: 94 percent / 10 percent NaOH / 5 h / Heating
2: thionyl chloride / cyclohexane / 6 h / Heating
View Scheme
参考文献
Mouysset, Genevieve; Payard, Marc; Grassy, Gerard; Tronche, Pierre; Dabire, Hubert; et al.
European Journal of Medicinal Chemistry, 1987 , vol. 22, p. 539 - 544
反应条件
1: 94.7 percent / 10percent NaOH / 5 h / Heating
2: SOCl2 / benzene / 3 h / Heating
View Scheme
参考文献
Gupta, R. C.; Pratap, Ram; Prasad, C. R.; Anand, Nitya
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 4 p. 344 - 347
反应条件
triethylamine in benzene
参考文献
Gupta, R. C.; Pratap, Ram; Prasad, C. R.; Anand, Nitya
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 4 p. 344 - 347
反应条件
triethylamine in benzene
参考文献
Gupta, R. C.; Pratap, Ram; Prasad, C. R.; Anand, Nitya
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 4 p. 344 - 347
反应条件
triethylamine in benzene
参考文献
Gupta, R. C.; Pratap, Ram; Prasad, C. R.; Anand, Nitya
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 4 p. 344 - 347
反应条件
triethylamine in benzene
参考文献
Gupta, R. C.; Pratap, Ram; Prasad, C. R.; Anand, Nitya
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 4 p. 344 - 347
反应条件
triethylamine in benzene
参考文献
Gupta, R. C.; Pratap, Ram; Prasad, C. R.; Anand, Nitya
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 4 p. 344 - 347