O-(叔丁基二甲基硅烷)羟胺合成路线 （共 10 条）
反应条件
hydroxylamine hydrochloride; ethylenediamine in dichloromethane T=20°C; 96 h;
参考文献
Organic and Biomolecular Chemistry, , vol. 4, # 22 p. 4178 - 4185
反应条件
in dichloromethane T=20°C; 15 h; Title compound not separated from byproducts;
参考文献
Alcazar, Jesus; Almena, Ines; Begtrup, Mikael; Hoz, Antonio de la
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 21 p. 2773 - 2782
反应条件
cycloocta-1,5-dienelt;(S)-1-(2-diphenylphosphino-1-naphthyl)isoquinolinegt;rhodium(I) trifluoromethanesulfonate; methyl-magnesium chloride; benzo[1,3,2]dioxaborole in tetrahydrofuran multistep reaction; other reagents, solvents; Product distribution;
参考文献
Knight, Frances I.; Brown, John M.; Lazzari, Dario; Ricci, Alfredo; Blacker, A. John
Tetrahedron, 1997 , vol. 53, # 33 p. 11411 - 11424
反应条件
cycloocta-1,5-dienelt;(S)-1-(2-diphenylphosphino-1-naphthyl)isoquinolinegt;rhodium(I) trifluoromethanesulfonate; methyl-magnesium chloride; benzo[1,3,2]dioxaborole in tetrahydrofuran multistep reaction; other reagents, solvents; Product distribution;
参考文献
Knight, Frances I.; Brown, John M.; Lazzari, Dario; Ricci, Alfredo; Blacker, A. John
Tetrahedron, 1997 , vol. 53, # 33 p. 11411 - 11424
反应条件
in N,N-dimethyl-formamide T=0 - 20°C; Inert atmosphere;
参考文献
Kitahara, Katsushi; Toma, Tatsuya; Shimokawa, Jun; Fukuyama, Tohru
Organic Letters, 2008 , vol. 10, # 11 p. 2259 - 2261
反应条件
tert-butyldimethylsilyl chloride in dichloromethane T=20°C; 15 h; Title compound not separated from byproducts;
参考文献
Alcazar, Jesus; Almena, Ines; Begtrup, Mikael; Hoz, Antonio de la
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 21 p. 2773 - 2782
反应条件
in dichloromethane T=20°C; 15 h; Title compound not separated from byproducts;
参考文献
Alcazar, Jesus; Almena, Ines; Begtrup, Mikael; Hoz, Antonio de la
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 21 p. 2773 - 2782
反应条件
cycloocta-1,5-dienelt;(S)-1-(2-diphenylphosphino-1-naphthyl)isoquinolinegt;rhodium(I) trifluoromethanesulfonate; methyl-magnesium chloride; benzo[1,3,2]dioxaborole in tetrahydrofuran
multistep reaction; other reagents, solvents; Product distribution;
参考文献
Knight, Frances I.; Brown, John M.; Lazzari, Dario; Ricci, Alfredo; Blacker, A. John
Tetrahedron, 1997 , vol. 53, # 33 p. 11411 - 11424
反应条件
1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine in dichloromethane
T=20°C; 16 h;
参考文献
Miller, Marvin J.; Zhao, Gaiying; Vakulenko, Sergei; Franzblau, Scott; Moellmann, Ute
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 22 p. 4178 - 4185
反应条件
cycloocta-1,5-dienelt;(S)-1-(2-diphenylphosphino-1-naphthyl)isoquinolinegt;rhodium(I) trifluoromethanesulfonate; methyl-magnesium chloride; benzo[1,3,2]dioxaborole in tetrahydrofuran
multistep reaction; other reagents, solvents; Product distribution;
参考文献
Knight, Frances I.; Brown, John M.; Lazzari, Dario; Ricci, Alfredo; Blacker, A. John
Tetrahedron, 1997 , vol. 53, # 33 p. 11411 - 11424
