1-甲基-2-(4-甲基苯基)磺酰基-苯合成路线 （共 20 条）
反应条件
iron(III) chloride
T=85 - 110°C;
参考文献
I.G. Farbenind.
Patent: DE701954 , 1938 ;
DRP/DRBP Org.Chem.
Full Text Show Details
Gen. Aniline and Film Corp.
Patent: US2224964 , 1939 ;
反应条件
In(OSO2CF3)3
T=120°C; 2 h; Title compound not separated from byproducts;
参考文献
Frost; Hartley; Whittle
Synlett, 2001 , # 6 p. 830 - 832
反应条件
in tetrahydrofuran
T=0 - 20°C;
参考文献
Dubbaka, Srinivas Reddy; Vogel, Pierre
Tetrahedron Letters, 2006 , vol. 47, # 20 p. 3345 - 3348
反应条件
1.1: neat (no solvent) / 20 °C
2.1: TPPD / dichloromethane / 0.5 h
2.2: 2 h / 0 - 20 °C
View Scheme
参考文献
Khodaei; Nazari
Journal of the Iranian Chemical Society, 2012 , vol. 9, # 4 p. 507 - 512
反应条件
in dichloromethane
T=0°C; 14 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Effenberger, Franz; Huthmacher, Klaus; Keil, Michael
Chemische Berichte, 1981 , vol. 114, # 5 p. 1967 - 1971
反应条件
dihydrogen peroxide; acetic acid
参考文献
Mody,M.K. et al.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1977 , vol. 15B, p. 1008 - 1012
反应条件
aluminum oxide; phosphorus pentoxide in water
Friedel-Crafts reaction; 1 h; Heating;
参考文献
Hajipour, Abdol R.; Zarei, Amin; Khazdooz, Leila; Pourmousavi, Seied A.; Mirjalili, Bi Bi F.; Ruoho
Phosphorus, Sulfur and Silicon and the Related Elements, 2005 , vol. 180, # 9 p. 2029 - 2034
反应条件
sulfuric acid; trifluoroacetic anhydride
Yield given. Yields of byproduct given;
参考文献
Tyobeka, Themba E.; Hancock, Richard A.; Weigel, Helmut
Journal of the Chemical Society, Chemical Communications, 1980 , # 3 p. 114 - 115
反应条件
(i) Mg, Et2O, (ii) /BRN= 1866906/, (iii) H2O2, AcOH; Multistep reaction;
参考文献
Kohara,Y. et al.
Bulletin of the Chemical Society of Japan, 1970 , vol. 43, p. 520 - 524
反应条件
Fe(3+)-montmorillonite
Substitution; Friedel-Crafts sulfonylation; 6 h; Heating; Product distribution; Further Variations:Reagents;
参考文献
Choudary, Boyapati M.; Chowdari, N. Sreenivasa; Kantam, M. Lakshmi
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 16 p. 2689 - 2693
