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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
反式-肉桂酸乙酯
合成路线
（共 451 条）
4192-77-2
反式-肉桂酸乙酯
→
反应条件
2021-28-5
3-苯丙酸乙酯
反应条件
tris(triphenylphosphine)ruthenium(II) chloride; sodium formate in water; 1,2-dichloro-benzene T=108.9°C; 0.166667 h;
参考文献
Oyamada, Hidekazu; Naito, Takeshi; Kobayashi, Shu
Beilstein Journal of Organic Chemistry, 2011 , vol. 7, art. no. 83, p. 735 - 739
4192-77-2
反式-肉桂酸乙酯
→
反应条件
2021-28-5
3-苯丙酸乙酯
+
501-52-0
3-苯基丙酸
反应条件
NaH-alkoxide-Ni salt reagent; water in tetrahydrofuran T=25°C; 0.25 h;
参考文献
Fort, Y.; Vanderesse, R.; Caubere, P.
Chemistry Letters, 1988 , # 5 p. 757 - 760
1066-35-9
二甲基一氯硅烷
+
4192-77-2
反式-肉桂酸乙酯
→
反应条件
2021-28-5
3-苯丙酸乙酯
+
1256931-30-2
反应条件
1: dimethylmono-chlorosilane With magnesium in N,N-dimethyl-formamide T=20°C; 0.25 h; Inert atmosphere; 2: benzalacetic acid ethyl ester in N,N-dimethyl-formamide T=30°C; 0.5 h; Inert atmosphere; 3: With water; sodium hydrogencarbonate in N,N-dimethyl-formamide CoolingSaturated solution; regiospecific reaction;
参考文献
Kundu, Pintu K.; Ghosh, Sunil K.
Tetrahedron, 2010 , vol. 66, # 44 p. 8562 - 8568
4028-23-3
烯丙基二甲基氯硅烷
+
4192-77-2
反式-肉桂酸乙酯
→
反应条件
2021-28-5
3-苯丙酸乙酯
+
1256931-29-9
反应条件
1: allyl(chloro)dimethylsilane With magnesium in N,N-dimethyl-formamide T=20°C; 0.25 h; Inert atmosphere; 2: benzalacetic acid ethyl ester in N,N-dimethyl-formamide T=30°C; 0.5 h; Inert atmosphere; 3: With water; sodium hydrogencarbonate in N,N-dimethyl-formamide CoolingSaturated solution; regiospecific reaction;
参考文献
Kundu, Pintu K.; Ghosh, Sunil K.
Tetrahedron, 2010 , vol. 66, # 44 p. 8562 - 8568
75-77-4
三甲基氯硅烷
+
4192-77-2
反式-肉桂酸乙酯
→
反应条件
2021-28-5
3-苯丙酸乙酯
+
35153-45-8
反应条件
1: chloro-trimethyl-silane With magnesium in N,N-dimethyl-formamide T=20°C; 0.25 h; Inert atmosphere; 2: benzalacetic acid ethyl ester in N,N-dimethyl-formamide T=30°C; 0.5 h; Inert atmosphere; 3: With water; sodium hydrogencarbonate in N,N-dimethyl-formamide CoolingSaturated solution; regiospecific reaction;
参考文献
Kundu, Pintu K.; Ghosh, Sunil K.
Tetrahedron, 2010 , vol. 66, # 44 p. 8562 - 8568
2372-33-0
+
4192-77-2
反式-肉桂酸乙酯
→
反应条件
2021-28-5
3-苯丙酸乙酯
+
1256931-27-7
反应条件
1: (p-methoxyphenyl)dimethylsilyl chloride With magnesium in N,N-dimethyl-formamide T=30°C; 0.25 h; Inert atmosphere; 2: benzalacetic acid ethyl ester in N,N-dimethyl-formamide T=20°C; 0.5 h; Inert atmosphere; 3: With water; sodium hydrogencarbonate in N,N-dimethyl-formamide CoolingSaturated solution; regiospecific reaction;
参考文献
Kundu, Pintu K.; Ghosh, Sunil K.
Tetrahedron, 2010 , vol. 66, # 44 p. 8562 - 8568
17881-63-9
+
4192-77-2
反式-肉桂酸乙酯
→
反应条件
2021-28-5
3-苯丙酸乙酯
+
1256931-41-5
反应条件
1: p-TolMe2SiCl With magnesium in N,N-dimethyl-formamide T=20°C; 0.25 h; Inert atmosphere; 2: benzalacetic acid ethyl ester in N,N-dimethyl-formamide T=30°C; 0.5 h; Inert atmosphere; 3: With water; sodium hydrogencarbonate in N,N-dimethyl-formamide CoolingSaturated solution; regiospecific reaction;
参考文献
Kundu, Pintu K.; Ghosh, Sunil K.
Tetrahedron, 2010 , vol. 66, # 44 p. 8562 - 8568
768-33-2
苯基二甲基氯硅烷
+
4192-77-2
反式-肉桂酸乙酯
→
反应条件
2021-28-5
3-苯丙酸乙酯
+
67263-05-2
反应条件
1: dimethyl(phenyl)silyl chloride With magnesium in N,N-dimethyl-formamide T=30°C; 0.25 h; Inert atmosphere; 2: benzalacetic acid ethyl ester in N,N-dimethyl-formamide T=20°C; 0.5 h; Inert atmosphere; 3: With water; sodium hydrogencarbonate in N,N-dimethyl-formamide CoolingSaturated solution; regiospecific reaction;
参考文献
Kundu, Pintu K.; Ghosh, Sunil K.
Tetrahedron, 2010 , vol. 66, # 44 p. 8562 - 8568
4192-77-2
反式-肉桂酸乙酯
→
反应条件
10094-36-7
环己基丙酸乙酯
+
2021-28-5
3-苯丙酸乙酯
反应条件
platinum-cathodes Electrolysis;
参考文献
Ono
J. electroch. Soc. Japan, 1955 , vol. 23, p. 117,118
108-24-7
乙酸酐
+
4192-77-2
反式-肉桂酸乙酯
→
反应条件
2021-28-5
3-苯丙酸乙酯
+
19449-94-6
+
63795-90-4
反应条件
tetrabutylammomium bromide in N,N-dimethyl-formamide T=25°C; electrochemical reduction; other activated olefins and acylating agents; var. electrodes, electrolytes and additive salts; var. current density; Product distributionMechanism;
参考文献
Tetrahedron, , vol. 52, # 6 p. 1943 - 1952
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