反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; Bu3SnLi
1.) THF, hexane, -78 deg C, 5 min, 2.) THF, hexane, -60 deg C to -50 deg C, 3 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Kusuda, Shinya; Ueno, Yoshio; Toru, Takeshi
Bulletin of the Chemical Society of Japan, 1993 , vol. 66, # 9 p. 2720 - 2724