1-(4-氟苯基)-3-苯基-1-丙酮合成路线 (共 13 条)
反应条件
1: [IrH(1,5-cyclooctadiene)Cl(HCN(i-Pr)CHCN(C2H4PPh2))]PF6; isopropyl alcohol; potassium hydroxide / 4 h / Inert atmosphere 2: [IrH(1,5-cyclooctadiene)Cl(HCN(i-Pr)CHCN(C2H4PPh2))]PF6; potassium hydroxide / toluene / 2 h / 110 °C / Inert atmosphere View Scheme
参考文献
Cho, Chan Sik; Kim, Bok Tae; Yoon, Nam Sik
Applied Organometallic Chemistry, 2011 , vol. 25, # 9 p. 695 - 698
反应条件
1: methanol; sodium tetrahydroborate 2: tris(triphenylphosphine)ruthenium(II) chloride; dodec-1-ene; potassium hydroxide / 1,4-dioxane / 40 h / 80 °C View Scheme
参考文献
Cho, Chan Sik; Kim, Bok Tae; Yoon, Nam Sik
Applied Organometallic Chemistry, 2011 , vol. 25, # 9 p. 695 - 698
反应条件
in ethanol T=15 - 35°C; polarographic reduction at the dropping mercury electrode at the different concentrations and pH; Mechanism;
参考文献
Katiyar, Sarvagya S.; Latithambica, M.
Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical & Analytical, 1980 , vol. 19, # 10 p. 956 - 960