反应条件
1: 4-dimethylamino-1-tert-butyldimethylsilyloxynaphthalene With tert.-butyl lithium in cyclohexane; pentane
T=20°C; 72 h;
2: N,N-dimethyl-formamide With sulfuric acid; iodine in cyclohexane; pentane
T=0 - 20°C;
3: With jones' reagent in acetone
T=0°C; Jones' oxidation; 0.5 h; Further stages.;
参考文献
Kraus, George A.; Kim, Junwon
Journal of Organic Chemistry, 2002 , vol. 67, # 7 p. 2358 - 2360