1: B-1-hexyldiphenylborane; p-benozquinone in diethyl ether
T=20°C; Inert atmosphere;
2: With water in diethyl ether
Inert atmosphere;
3: ethanolamine Inert atmosphereCooling with ice; regioselective reaction;
参考文献
Zillman, David J.; Hincapie, Gloria C.; Reza Savari; Mizori, Farhad G.; Cole, Thomas E.
Tetrahedron Letters, 2010 , vol. 51, # 23 p. 3033 - 3036