N,N,1-三甲基-1H-吲哚-2-甲酰胺合成路线 （共 5 条）
反应条件
1,3-Diiodo-5,5-dimethyl-2,4-imidazolidinedione; potassium carbonate in tetrachloromethane; water
T=20°C; Inert atmosphere;
参考文献
Baba, Haruka; Moriyama, Katsuhiko; Togo, Hideo
Synlett, 2012 , vol. 23, # 8 p. 1175 - 1180
反应条件
thionyl chloride; benzene
Behandeln des Reaktionsprodukts mit Dimethylamin in Aether;
参考文献
Snyder; Cook
Journal of the American Chemical Society, 1956 , vol. 78, p. 969,971
反应条件
1: 90 percent / methanol; H2O / 15 h / Ambient temperature
2: 1) LDA / 1) THF, -70 deg C, 30 min., 2) -30 deg C, 2 h
View Scheme
参考文献
Bennasar, M.-Lluisa; Zulaica, Ester; Bosch, Joan
Journal of Organic Chemistry, 1992 , vol. 57, # 10 p. 2835 - 2841
反应条件
lithium diisopropyl amide
1) THF, -70 deg C, 30 min., 2) -30 deg C, 2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Bennasar, M.-Lluisa; Zulaica, Ester; Bosch, Joan
Journal of Organic Chemistry, 1992 , vol. 57, # 10 p. 2835 - 2841
反应条件
lithium diisopropyl amide
1) THF, -70 deg C, 30 min., 2) -30 deg C, 2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Bennasar, M.-Lluisa; Zulaica, Ester; Bosch, Joan
Journal of Organic Chemistry, 1992 , vol. 57, # 10 p. 2835 - 2841
