2-[(4-甲氧基苯基)亚氨基]-1,2-二苯基乙酮合成路线 (共 11 条)
反应条件
potassium hexacyanoferrate(III) in ethanol; water; benzene
T=70°C; 3.5 h;
参考文献
Van Belzen, Ruud; Klein, Rene A.; Smeets, Wilberth J.J.; Spek, Anthony L.; Benedix, Roland; Elsevier, Cornelis J.
Recueil des Travaux Chimiques des Pays-Bas-Journal of the Royal Netherlands, 1996 , vol. 115, # 5 p. 275 - 285
反应条件
1-amino-1-phenylethane; zinc(II) chloride in xylene
6 h; Heating;
参考文献
Alcaide, Benito; Lopez-Mardomingo, Carmen; Perez-Ossorio, Rafael; Plumet, Joaquin
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , # 11 p. 1649 - 1654
反应条件
1: 73 percent / 12M HCl / H2O / 3 h / 140 °C
2: 67 percent / K3Fe(CN)6 / benzene; ethanol; H2O / 3.5 h / 70 °C
View Scheme
参考文献
Van Belzen, Ruud; Klein, Rene A.; Smeets, Wilberth J.J.; Spek, Anthony L.; Benedix, Roland; Elsevier, Cornelis J.
Recueil des Travaux Chimiques des Pays-Bas-Journal of the Royal Netherlands, 1996 , vol. 115, # 5 p. 275 - 285
反应条件
1: 73 percent / 12M HCl / H2O / 3 h / 140 °C
2: 67 percent / K3Fe(CN)6 / benzene; ethanol; H2O / 3.5 h / 70 °C
View Scheme
参考文献
Van Belzen, Ruud; Klein, Rene A.; Smeets, Wilberth J.J.; Spek, Anthony L.; Benedix, Roland; Elsevier, Cornelis J.
Recueil des Travaux Chimiques des Pays-Bas-Journal of the Royal Netherlands, 1996 , vol. 115, # 5 p. 275 - 285
反应条件
(i) benzene, (ii) Et3N; Multistep reaction;
参考文献
Oka,K.; Hara,S.
Tetrahedron Letters, 1977 , p. 2939 - 2942
反应条件
TiI4 in acetonitrile
T=0 - 20°C; 30 h;
参考文献
Shimizu, Makoto; Sahara, Tetsuya; Hayakawa, Ryuuichirou
Chemistry Letters, 2001 , # 8 p. 792 - 793
反应条件
dicobalt octacarbonyl in tetrahydrofuran
T=60°C; P=760 Torr; 24 h;
参考文献
Alper, Howard; Amaratunga, Shiyamalie
Journal of Organic Chemistry, 1982 , vol. 47, # 18 p. 3593 - 3595
反应条件
in tetrahydrofuran
T=60°C; 7 h;
参考文献
Alper, Howard; Amaratunga, Shiyamaline
Tetrahedron Letters, 1981 , vol. 22, # 39 p. 3811 - 3812
反应条件
triethylamine in toluene
24 h; Heating;
参考文献
Alcaide; Leon-Santiago; Perez-Ossorio; et al.
Synthesis, 1982 , vol. No. 11, p. 989 - 990
参考文献
Alcaide, Benito; Dominguez, Gema; Plumet, Joaquin; Sierra, Miguel A.
Heterocycles, 1988 , vol. 27, # 6 p. 1317 - 1320