5-硝基-1,10-菲咯啉合成路线 （共 16 条）
反应条件
sodium hydroxide T=90 - 100°C; 0.333333 h;
参考文献
Gillard, R. D.; Houghton, Roy P.; Tucker, John N.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1980 , p. 2102 - 2107
反应条件
potassium hydroxide; sodium tetrahydroborate; sulfuric acid; nitric acid 1) 80 deg C, 2.5 h, 2b) 120-130 deg C, 2 h; Yield given. Multistep reaction;
参考文献
Torieda, Hiroaki; Nozaki, Koichi; Yoshimura, Akio; Ohno, Takeshi
Journal of Physical Chemistry A, 2004 , vol. 108, # 22 p. 4819 - 4829
反应条件
1: hydroxylamine hydrochloride / ethanol / Heating View Scheme
参考文献
Camren, Heather; Chang, Mei-Yueh; Zeng, Liansheng; McGuire, Mark E.
Synthetic Communications, 1996 , vol. 26, # 6 p. 1247 - 1252
反应条件
potassium hydroxide; hydroxylamine hydrochloride in 1,4-dioxane; methanol; ethanol T=4 - 20°C; 2 h;
参考文献
Ghosh, Amrita; Mandoli, Amit; Kumar, D. Krishna; Yadav, Narendra Singh; Ghosh, Tamal; Jha, Bhavanath; Thomas, Jim A.; Das, Amitava
Dalton Transactions, 2009 , # 42 p. 9312 - 9321
反应条件
in ethanol; acetonitrile
dropwise addn. of soln. of Ln(ClO4)2 (in EtOH) and sol. of nitrophenanthroline (in MeCN) to soln. of isophthalate (in EtOH) (stirring), refluxing (18 h; pptn.); filtration, washing (EtOH, MeCN, Me2O), drying (over P2O5, vac.), recrystn. (DMF/EtOH 2 : 1); elem. anal.;
参考文献
Li, Yan-Tuan; Yan, Cui-Wei; Yi, Nie
Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry, 1999 , vol. 29, # 7 p. 1153 - 1169
反应条件
1: H2 / Pd/C / N,N-dimethyl-acetamide / 48 h
2: 1.18 g / sodium acetate / N,N-dimethyl-acetamide; H2O; acetone / 0.08 h
View Scheme
参考文献
Khimich; Obrezkov; Koptelova
Russian Journal of Organic Chemistry, 2006 , vol. 42, # 4 p. 555 - 557
