1: 68 percent / Br2, NaOH / 2 h / 5 °C 2: 97 percent / 5 h / Heating View Scheme

1: 64 percent / Br2; NaOH 2: thionyl chloride View Scheme

暂无反应条件数据

sodium azide; [bis(acetoxy)iodo]benzene in acetonitrile T=6 - 10°C; 24 h; Inert atmosphere;

1: 1-Bromo-3-iodopropane With indium; copper(l) chloride in tetrahydrofuran T=20°C; 24 h; 2: 4'-iodoacetophenone With bis-triphenylphosphine-palladium(II) chloride; lithium chloride in N,N-dimethyl acetamide T=100°C; 24 h;

1: acetic anhydride With AlCl3, aluminium chloride in dichloromethane Friedel Crafts acylation; 0.75 h; Inert atmosphereCooling with ice; 2: 1-bromo-3-phenyl-propane in dichloromethane 2.5 h; Inert atmosphereCooling with ice; 3: With hydrogenchloride in dichloromethane; water

1: methanol; sodium tetrahydroborate / 2 h / Inert atmosphere; Cooling with ice 2: toluene-4-sulfonic acid / toluene / 3 h / Inert atmosphere; Reflux View Scheme

sodium hydroxide; bromine in 1,4-dioxane T=20°C; 1 h;