Costa De Souza, Marcos; Pires De Macedo, William; Campos M. Da Silva, Marcelo; Costa De O. Ramos, Guilherme; Alt, Helmut G.
Phosphorus, Sulfur and Silicon and the Related Elements, 2004 , vol. 179, # 6 p. 1047 - 1054
1: Carbamonitrile; Allyl isothiocyanate With potassium hydroxide in ethanol
T=20°C; 1 h;
2: ethyl alpha-chloroacetoacetate With potassium hydroxide in ethanol
0.5 h; Reflux;
3: With hydrogenchloride in ethanol; water
T=20°C; pH=7; regioselective reaction;
参考文献
Shestopalov, Anatoliy M.; Rodinovskaya, Liudmila A.; Shestopalov, Alexander A.
Tetrahedron, 2010 , vol. 66, # 46 p. 8945 - 8948
in neat (no solvent)
Electric Arc; O2 at ca. 3 atm expansion through pulsed molecular beam valve into reservoir with H2NCN and finally through pulsed electric discharge, accordingto T. R. Taylor et al., Chem. Phys. Lett. 301 (1999) 413; negative ions acceleration to 8 keV and sepn. temporally by Bakker TOF mass spectrometer;
参考文献
Bise, Ryan T.; Choi, Hyeon; Neumark, Daniel M.
Journal of Chemical Physics, 1999 , vol. 111, # 11 p. 4923 - 4932
