in neat (no solvent) (CH3)3SiCl and ZnF2 (dried at 110°C for 24 h) under formation of gas;;
参考文献
Newkirk, A. E.
Journal of the American Chemical Society, 1946 , vol. 68, p. 2736 - 2737
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Gmelin Handbook: Si: MVol.C, 37, page 115 - 117