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in neat (no solvent, solid phase) thermolysis at 520°C (<0.005 Torr); cooling to -183°C, warming to -78°C with addn. of pentane, evapn. at -30°C (vac.), distn. (vac.) and recryst. from pentaneat -80°C;
参考文献
Boese, Roland; Paetzold, Peter; Tapper, Alexander
Chemische Berichte, 1987 , vol. 120, p. 1069 - 1072
in decane addn. of a soln. of Me3SiNHC6H5 in decane to 2,4,6-tri-t-butylphenyl difluoroborane and vigorously refluxing for 3-5 d under N2; distilling off the excess of amine and fractional distn. of the phenylaminoborane from the residue, elem. anal.;
参考文献
Geschwentner, M.; Elter, G.; Meller, A.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1993 , vol. 619, p. 1474 - 1478
