in monofluoro-trichloromethane onto a frozen soln. of Me3SiNMe2 in CFCl3 in an NMR-tube BF3 is condensed at -196°C, warming up to room temp.; monitored by NMR-spectroscopy;
参考文献
Tornieporth-Oetting, I. C.; Klapoetke, T. M.
Polyhedron, 1992 , vol. 11, p. 2183 - 2186
Messdoerffer, J. N.; Niederpruem, H.
Chemiker-Zeitung, 1972 , vol. 96, p. 582 - 583
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Gmelin Handbook: F: PerFHalOrg.2, 1.3.3, page 120 - 137
fluoride gas-phase reaction; gas-phase reactions of anions with substituted silanes; Product distribution;
参考文献
DePuy, C. H.; Bierbaum, Veronica M.; Flippin, L. A.; Grabowski, Josef J.; King, Gary K.; et al.
Journal of the American Chemical Society, 1980 , vol. 102, # 15 p. 5012 - 5015
fluoride gas-phase reaction; gas-phase reactions of anions with substituted silanes; Product distribution;
参考文献
DePuy, C. H.; Bierbaum, Veronica M.; Flippin, L. A.; Grabowski, Josef J.; King, Gary K.; et al.
Journal of the American Chemical Society, 1980 , vol. 102, # 15 p. 5012 - 5015
