1-氯-2,2-二氟丙烷合成路线 （共 22 条）
反应条件
hydrogen fluoride; diphenylamine T=122°C;
参考文献
ASAHI GLASS COMPANY, LIMITED
Patent: US2011/237846 A1, 2011 ;
Location in patent: Page/Page column 5 ;
反应条件
hydrogen fluoride T=95°C;
参考文献
Henne; Arnold
Journal of the American Chemical Society, 1948 , vol. 70, p. 759
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Henne; Plueddeman
Journal of the American Chemical Society, 1943 , vol. 65, p. 1272
反应条件
hydrogen fluoride T=50 - 60°C;
参考文献
Henne; Haeckl
Journal of the American Chemical Society, 1941 , vol. 63, p. 2692
反应条件
hydrogen fluoride; mercury(II) oxide T=25°C;
参考文献
Henne; Flanagan
Journal of the American Chemical Society, 1943 , vol. 65, p. 2362
反应条件
bromine trifluoride; tin(IV) chloride in 1,2,2-trifluoro-trichloroethane T=20 - 25°C;
参考文献
Kartashov, A. V.; Chuvatkin, N. N.; Boguslavskaya, L. S.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 12 p. 2276 - 2278
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 12 p. 2522 - 2525
反应条件
hydrogen fluoride T=50 - 60°C; 12 h; Further byproducts given;
参考文献
Fainberg,A.H.; Miller,W.T.
Journal of Organic Chemistry, 1965 , vol. 30, p. 864 - 876
反应条件
hydrogen fluoride; fluoro chloride T=-30 - -15°C;
参考文献
Chuvatkin, N. N.; Panteleeva, I. Yu.; Boguslavskaya, L. S.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, # 5 p. 821 - 827
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 5 p. 946 - 953
反应条件
sulfur(IV) fluoride; hydrogen fluoride; chlorine T=75°C; 5 h; stainless-steel autoclave; Yield given;
参考文献
Muratov, N. N.; Omarov, V. O.; Kunshenko, B. V.; Burmakov, A. I.; Alekseeva, L. A.; Yagupol'skii, L. M.
Journal of Organic Chemistry USSR (English Translation), 1986 , vol. 22, # 9 p. 1621 - 1626
Zhurnal Organicheskoi Khimii, 1986 , vol. 22, # 9 p. 1806 - 1812
反应条件
fluoro chloride T=-120 - -10°C; 12 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Arimura, Takashi; Kurosawa, Shigeru; Sekiya, Akira
Chemistry Letters, 1993 , # 1 p. 35 - 36
反应条件
fluoro chloride T=-120 - -10°C; 12 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Arimura, Takashi; Kurosawa, Shigeru; Sekiya, Akira
Chemistry Letters, 1993 , # 1 p. 35 - 36
