4-叔丁基-2,6-二甲基苯胺合成路线 （共 9 条）
反应条件
Fe-HCl in ethanol; water 28 h; Heating;
参考文献
Osuka, Atsuhiro; Shimizu, Hirohito; Suzuki, Hitomi
Chemistry Letters, 1983 , p. 1373 - 1374
反应条件
1: AlCl3-MeNO2 2: 75 percent / acetic anhydride, nitric acid, acetic acid / 25 °C 3: 89 percent / Fe-HCl / H2O; ethanol / 28 h / Heating View Scheme
参考文献
Yamato, Takehiko; Arimura, Takashi; Tashiro, Masashi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1 - 8
反应条件
(i) NO2/HNO3, Ac2O, AcOH, (ii) (reduction); Multistep reaction;
参考文献
Small, Brooke L.; Rios, Ray; Fernandez, Eric R.; Gerlach, Deidra L.; Halfen, Jason A.; Carney, Michael J.
Organometallics, 2010 , vol. 29, # 24 p. 6723 - 6731
反应条件
sulfuric acid; nitric acid
参考文献
Baur
Chemische Berichte, 1900 , vol. 33, p. 2564
反应条件
1: 48 percent / HBF4, NaNO2 / tetrahydrofuran; H2O 2: 89.9 percent / biphenyl / AlCl3 / CS2 / 1.5 h / Ambient temperature View Scheme
参考文献
Yamato, Takehiko; Arimura, Takashi; Tashiro, Masashi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1 - 8
反应条件
sulfuric acid; sodium nitrite
Kochen der erhaltenen Diazoniumsalz-Loesung;
参考文献
Tchitchibabine
Bulletin de la Societe Chimique de France, 1932 , vol. <4> 51, p. 1436,1441
反应条件
hydrogenchloride
Diazotization.Eintragen in ein Gemisch von wss. Alkali-tetracyanocuprat(I)-Loesung und Benzol;
参考文献
Fuson et al.
Journal of Organic Chemistry, 1947 , vol. 12, p. 587,592
反应条件
1: Diazotization
2: pyridine / 220 °C
3: fuming sulfuric acid; nitric acid / 3 °C
View Scheme
参考文献
Fuson et al.
Journal of Organic Chemistry, 1947 , vol. 12, p. 587,592
参考文献
Fuson et al.
Journal of Organic Chemistry, 1947 , vol. 12, p. 587,592
