6-叔-丁基-1,2,3,4-四氢萘合成路线 (共 5 条)
反应条件
aluminum tri-bromide
T=120 - 130°C;
参考文献
Barbot
Bulletin de la Societe Chimique de France, 1930 , vol. <4> 47, p. 1314,1318
Full Text Show Details
Whitmore; James
Journal of the American Chemical Society, 1943 , vol. 65, p. 2088
反应条件
T=300°C; P=20594.2 Torr; Leiten ueber Aluminiumoxyd-Siliciumdioxyd-Kontakte;
参考文献
Kutz et al.
Journal of the American Chemical Society, 1948 , vol. 70, p. 4026,4030
反应条件
zinc(II) chloride
T=75 - 110°C; 6 h;
参考文献
Jackson, Richard A.; Rhodes, Christopher J.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1993 , # 1 p. 53 - 57
反应条件
1: 20 percent / glacial AcOH, 85percent H3PO4, concd HCl / 6 h / Heating
2: 98 percent / LiAlH4 / tetrahydrofuran / 4 h / Heating
3: 75 percent / sulfur / 1.58 h / 230 - 270 °C
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参考文献
Jackson, Richard A.; Rhodes, Christopher J.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1993 , # 1 p. 53 - 57
反应条件
chromium(VI) oxide; acetic acid
参考文献
Burnham,J.W. et al.
Journal of Organic Chemistry, 1974 , vol. 39, # 10 p. 1416 - 1420