3-(乙基氨基)-1-丙醇合成路线 (共 8 条)
反应条件
in benzene 4 h; Heatingremoval of water;
参考文献
Katritzky, Alan R.; Baker, Victor J.; Brito-Palma, Fernando M. S.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1980 , p. 1739 - 1745
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
48 h; Heating / reflux;
参考文献
American Home Products Corporation
Patent: US6340687 B1, 2002 ;
Location in patent: Example 3 ;
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
参考文献
Katritzky, Alan R.; Baker, Victor J.; Brito-Palma, Fernando M. S.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1980 , p. 1739 - 1745
反应条件
hydrogen; nickel in ethanol
参考文献
Schloegl,K.; Schloegl,R.
Monatshefte fuer Chemie, 1964 , vol. 95, p. 922 - 941
参考文献
Goldberg; Whitmore
Journal of the American Chemical Society, 1937 , vol. 59, p. 2280
参考文献
Bottini; Roberts
Journal of the American Chemical Society, 1958 , vol. 80, p. 5203,5208
反应条件
acrylic acid sodium salt
T=120 - 150°C;
参考文献
Kurihara et al.
Yakugaku Zasshi, 1954 , vol. 74, p. 763
Chem.Abstr., 1955 , p. 11646
反应条件
NaOD; sodium salt of phosphorous acid in acetonitrile-D3; water-d2
T=25°C; 5 h; Product distribution;
参考文献
Schmidt; Schmidt, Brigitte F.; Snyder; Snyder, Emily J.; Carroll; Carroll, Robin M.; Farnsworth; Farnsworth, David W.; Michejda; Michejda, Christopher J.; Smith R.H.; Smith Jr., Richard H.
Journal of Organic Chemistry, 1997 , vol. 62, # 25 p. 8660 - 8665