3-甲酰基-7-甲氧基色酮合成路线 （共 3 条）
反应条件
1: N,N-dimethyl-formamide With bis(trichloromethyl) carbonate in 1,2-dichloro-ethane
T=0 - 20°C;
2: 2'-hydroxy-4'-methoxy acetophenone in 1,2-dichloro-ethane
T=0 - 20°C; 3.5 h; Further stages.;
参考文献
Su; Li; Zhao
Organic Preparations and Procedures International, 2007 , vol. 39, # 5 p. 495 - 502
参考文献
Qi, Gao-Fei; Yang, Zheng-Yin; Qin, Dong-Dong
Chemical and Pharmaceutical Bulletin, 2009 , vol. 57, # 1 p. 69 - 73
反应条件
1: acetic anhydride; boron trifluoride diethyl etherate / 1 h / 100 °C
2: trichlorophosphate / 1 h / 100 °C
View Scheme
参考文献
Fan, Long; Li, Tian-Rong; Wang, Bao-Dui; Yang, Zheng-Yin; Liu, Chun-Jiao
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 2014 , vol. 118, p. 760 - 764
