6,8-二溴-3-甲酰色酮合成路线 (共 2 条)
反应条件
1: N,N-dimethyl-formamide With bis(trichloromethyl) carbonate in 1,2-dichloro-ethane T=0 - 20°C; 2: 3',5'-dibromo-2'-hydroxyacetophenone in 1,2-dichloro-ethane T=0 - 20°C; 4.5 h; Further stages.;
参考文献
Su; Li; Zhao
Organic Preparations and Procedures International, 2007 , vol. 39, # 5 p. 495 - 502
反应条件
trichlorophosphate 24 h; Ambient temperature;
参考文献
Cascaval, Alexandru
Liebigs Annalen der Chemie, 1980 , # 5 p. 669 - 672