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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
氯苯基硅烷
合成路线
（共 31 条）
4206-75-1
氯苯基硅烷
→
反应条件
27484-20-4
+
50518-29-1
+
694-53-1
苯硅烷
+
775-12-2
二苯基硅烷
反应条件
Mg-anode; stainless steel cathode in tetrahydrofuran 29 h; Electrolysis;
参考文献
Grogger, Christa; Loidl, Bernhard; Stueger, Harald; Kammel, Thomas; Pachaly, Bernd
Journal of Organometallic Chemistry, 2006 , vol. 691, # 1-2 p. 105 - 110
4206-75-1
氯苯基硅烷
+
13406-07-0
→
反应条件
4314-98-1
反应条件
1: 1-methylpentylmagnesiumbromide With tributylphosphine; iron(III) chloride; copper(I) bromide in tetrahydrofuran T=-25°C; 0.166667 h; 2: phenyl-chloro-silane in tetrahydrofuran T=30°C; Grignard reaction; 2 h; Further stages.;
参考文献
Shirakawa, Eiji; Ikeda, Daiji; Yamaguchi, Shigeru; Hayashi, Tamio
Chemical Communications, 2008 , # 10 p. 1214 - 1216
4206-75-1
氯苯基硅烷
→
反应条件
4314-98-1
反应条件
in tetrahydrofuran; diethyl ether T=30°C; Grignard reaction;
参考文献
Shirakawa, Eiji; Ikeda, Daiji; Yamaguchi, Shigeru; Hayashi, Tamio
Chemical Communications, 2008 , # 10 p. 1214 - 1216
592-41-6
1-己烯
+
4206-75-1
氯苯基硅烷
+
33240-34-5
环戊基溴化镁
→
反应条件
4314-98-1
反应条件
1: 1-hexene With anhydrous iron chloride; tributylphosphine; copper(I) bromide in diethyl ether T=-20°C; 0.0833333 h; Inert atmosphere; 2: c-PentMgBr in diethyl ether T=-20°C; 1 h; Inert atmosphere; 3: phenyl-chloro-silane in diethyl ether T=30°C; 2 h; Inert atmosphere;
参考文献
Shirakawa, Eiji; Ikeda, Daiji; Masui, Seiji; Yoshida, Masatoshi; Hayashi, Tamio
Journal of the American Chemical Society, 2012 , vol. 134, # 1 p. 272 - 279
4206-75-1
氯苯基硅烷
+
3761-92-0
己基溴化镁
→
反应条件
4314-98-1
反应条件
in diethyl ether T=30°C; 2 h; Inert atmosphere;
参考文献
Shirakawa, Eiji; Ikeda, Daiji; Masui, Seiji; Yoshida, Masatoshi; Hayashi, Tamio
Journal of the American Chemical Society, 2012 , vol. 134, # 1 p. 272 - 279
68941-76-4
溴(3-己烷基)镁
+
4206-75-1
氯苯基硅烷
→
反应条件
反应条件
1: 1-ethylbutylmagnesium bromide With anhydrous iron chloride; tributylphosphine; copper(I) bromide in tetrahydrofuran; diethyl ether T=-25°C; 0.166667 h; Inert atmosphere; 2: phenyl-chloro-silane in tetrahydrofuran; diethyl ether T=30°C; 2 h; Inert atmosphere;
参考文献
Shirakawa, Eiji; Ikeda, Daiji; Masui, Seiji; Yoshida, Masatoshi; Hayashi, Tamio
Journal of the American Chemical Society, 2012 , vol. 134, # 1 p. 272 - 279
592-41-6
1-己烯
+
4206-75-1
氯苯基硅烷
+
927-77-5
丙基溴化镁
→
反应条件
4314-98-1
+
17882-13-2
反应条件
1: 1-hexene With anhydrous iron chloride; tributylphosphine; copper(I) bromide in diethyl ether T=-20°C; 0.0833333 h; Inert atmosphere; 2: n-propyl-magnesium bromide in diethyl ether T=-20°C; 1 h; Inert atmosphere; 3: phenyl-chloro-silane in diethyl ether T=30°C; 2 h; Inert atmosphere;
参考文献
Shirakawa, Eiji; Ikeda, Daiji; Masui, Seiji; Yoshida, Masatoshi; Hayashi, Tamio
Journal of the American Chemical Society, 2012 , vol. 134, # 1 p. 272 - 279
592-41-6
1-己烯
+
4206-75-1
氯苯基硅烷
+
931-50-0
环己基溴化镁
→
反应条件
4314-98-1
+
18036-87-8
反应条件
1: 1-hexene With anhydrous iron chloride; tributylphosphine; copper(I) bromide in diethyl ether T=-20°C; 0.0833333 h; Inert atmosphere; 2: cyclohexyl magnesium bromide in diethyl ether T=-20°C; 1 h; Inert atmosphere; 3: phenyl-chloro-silane in diethyl ether T=30°C; 2 h; Inert atmosphere;
参考文献
Shirakawa, Eiji; Ikeda, Daiji; Masui, Seiji; Yoshida, Masatoshi; Hayashi, Tamio
Journal of the American Chemical Society, 2012 , vol. 134, # 1 p. 272 - 279
592-41-6
1-己烯
+
4206-75-1
氯苯基硅烷
+
4852-26-0
3-戊基溴化镁
→
反应条件
1351520-92-7
+
17988-45-3
+
4314-98-1
反应条件
1: 1-hexene With anhydrous iron chloride; tributylphosphine; copper(I) bromide in diethyl ether T=-20°C; 0.0833333 h; Inert atmosphere; 2: 3-pentylmagnesium bromide in diethyl ether T=-20°C; 1 h; Inert atmosphere; 3: phenyl-chloro-silane in diethyl ether T=30°C; 2 h; Inert atmosphere;
参考文献
Shirakawa, Eiji; Ikeda, Daiji; Masui, Seiji; Yoshida, Masatoshi; Hayashi, Tamio
Journal of the American Chemical Society, 2012 , vol. 134, # 1 p. 272 - 279
68941-76-4
溴(3-己烷基)镁
+
872-05-9
1-癸烯
+
4206-75-1
氯苯基硅烷
→
反应条件
反应条件
1: 1-n-decene With anhydrous iron chloride; tributylphosphine; copper(I) bromide in tetrahydrofuran T=-25°C; 0.0833333 h; Inert atmosphere; 2: 1-ethylbutylmagnesium bromide in tetrahydrofuran; diethyl ether T=-25°C; 0.166667 h; Inert atmosphere; 3: phenyl-chloro-silane in tetrahydrofuran; diethyl ether T=30°C; 2 h; Inert atmosphere;
参考文献
Shirakawa, Eiji; Ikeda, Daiji; Masui, Seiji; Yoshida, Masatoshi; Hayashi, Tamio
Journal of the American Chemical Society, 2012 , vol. 134, # 1 p. 272 - 279
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