5-氯-2,2-二甲基戊腈合成路线 （共 13 条）
反应条件
2,2'-azo-bisisobutyronitrile in toluene
T=41.85°C; Addition; Photolysis; Kinetics;
参考文献
Heberger; Fischer
International Journal of Chemical Kinetics, 1993 , vol. 25, # 4 p. 249 - 263
反应条件
1: ethane-1,2-diol
2: (i) NaNH2, Et2O, (ii) H2SO4, AcOH
3: (i) Br2, Et2O, (ii) /BRN= 3964865/, MeOH
4: aq. H2O2 / acetic acid
View Scheme
参考文献
Truce,W.E. et al.
Journal of Organic Chemistry, 1962 , vol. 27, p. 2821 - 2828
反应条件
diisobutylaluminium hydride in dichloromethane
参考文献
Coldham, Iain; Jana, Samaresh; Watson, Luke; Pilgram, Christopher D.
Tetrahedron Letters, 2008 , vol. 49, # 37 p. 5408 - 5410
