(S)-(+)-3-甲基-1-戊醇合成路线 (共 30 条)
反应条件
lithium aluminium tetrahydride in diethyl ether 72 h; Heating;
参考文献
Baar, Cliff R.; Levy, Christopher J.; Min, Endy Y.-J.; Henling, Lawrence M.; Day, Michael W.; Bercaw, John E.
Journal of the American Chemical Society, 2004 , vol. 126, # 26 p. 8216 - 8231
反应条件
lithium aluminium tetrahydride in diethyl ether
参考文献
Chattopadhyay; Chadha; Mamdapur
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1991 , vol. 30, # 2 p. 247 - 249
反应条件
lithium aluminium tetrahydride in diethyl ether
参考文献
Chen, Zhiyong; Ye, Tao
Synlett, 2005 , # 18 art. no. W01405ST, p. 2781 - 2785
反应条件
1.1: NaNO2; HBr / 12 h / 0 - 20 °C 1.2: 65 percent / Zn; H2SO4 / 12 h / 0 - 20 °C 2.1: 70 percent / H2SO4 / 12 h / Heating 3.1: LiAlH4 / diethyl ether / 3 h / 20 °C View Scheme
参考文献
Baar, Cliff R.; Levy, Christopher J.; Min, Endy Y.-J.; Henling, Lawrence M.; Day, Michael W.; Bercaw, John E.
Journal of the American Chemical Society, 2004 , vol. 126, # 26 p. 8216 - 8231
反应条件
sodium tetrahydroborate in tetrahydrofuran; ethanol T=0 - 20°C;
参考文献
Zhou; Lu; Chen; Yang
Chemistry of Natural Compounds, 2010 , vol. 46, # 1 p. 83 - 85
反应条件
1: 44 percent / 0.1 M phosphate buffer / 53 h / Ambient temperature; hog liver carboxylesterase catalyzed transesterification 2: H2O, KCl / acetone View Scheme
参考文献
Cambou, Bernard; Klibanov, Alexander M.
Journal of the American Chemical Society, 1984 , vol. 106, # 9 p. 2687 - 2692
反应条件
hydrogen; palladium on activated charcoal
参考文献
Mori, Kenji; Sugai, Takeshi
Synthesis, 1982 , # 9 p. 752 - 753
反应条件
lithium aluminium tetrahydride in diethyl ether T=20°C; 3 h;
参考文献
Kumaraswamy; Markondaiah
Tetrahedron Letters, 2007 , vol. 48, # 10 p. 1707 - 1709
反应条件
1: Zn; aq. H2SO4 2: 100 percent / LiAlH4 / diethyl ether View Scheme
参考文献
Igarashi, Yasuhiro; Yanase, Saeko; Sugimoto, Kohei; Enomoto, Masaru; Miyanaga, Satoshi; Trujillo, Martha E.; Saiki, Ikuo; Kuwahara, Shigefumi
Journal of Natural Products, 2011 , vol. 74, # 4 p. 862 - 865
参考文献
Pino et al.
Journal of Organic Chemistry, 1959 , vol. 24, p. 1399,1403