Knunyantz,U.L. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1966 , p. 972 - 976
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Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, # 4 p. 626 - 630
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 4 p. 718 - 723
in further solvent(s) Os complex suspd. in tetraglyme under vac., CF3COOH distd. into react. vessel on vac. line (molar ratio 1:1), mixt. stirred at room temp. for 2h, 2 equiv of FSO3CH3 distd. into react. vessel, mixt. stirred at room temp. for 2 h; mixt. of product and CF3COOCH3 distd. into -196°C cold trap, redistd. through -63°C bath, dried over P2O5;
参考文献
Carter, Willie J.; Kelland, John W.; Okrasinski, Stanley J.; Warner, Keith E.; Norton, Jack R.
Inorganic Chemistry, 1982 , vol. 21, p. 3955 - 3960