反应条件
in dichloromethane N2-atmosphere, room temp.; stirring of mixt. of Fe-complexes with excessFSO2OMe for 1 h, addn. of excess NaBH4, stirring for 1 h; solvent removal, chromy. (Al2O3, CH2Cl2/hexane=1:1, then CH2Cl2);
参考文献
Goddard, Richard; Killops, Stephen D.; Knox, Selby A. R.; Woodward, Peter
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1978 , p. 1255 - 1260