1-(叔丁氧基羰基)-2-苯肼合成路线 （共 21 条）
反应条件
1: NH4OH / ethanol
2: (CF3CO)2O / pyridine
3: CH2Cl2
View Scheme
参考文献
Carpino,L.A.
Journal of the American Chemical Society, 1960 , vol. 82, p. 2725 - 2727
反应条件
1: 100 percent / tetrahydrofuran / 24 h / Heating
2: 40 percent / Oxone(R); NaHCO3 / acetonitrile; H2O / 23 h / 20 °C
3: 55 percent / toluene / 72 h / 20 °C
View Scheme
参考文献
Armstrong, Alan; Jones, Lyn H.; Knight, Jamie D.; Kelsey, Richard D.
Organic Letters, 2005 , vol. 7, # 4 p. 713 - 716
反应条件
1: 40 percent / Oxone(R); NaHCO3 / acetonitrile; H2O / 23 h / 20 °C
2: 55 percent / toluene / 72 h / 20 °C
View Scheme
参考文献
Armstrong, Alan; Jones, Lyn H.; Knight, Jamie D.; Kelsey, Richard D.
Organic Letters, 2005 , vol. 7, # 4 p. 713 - 716
参考文献
Carpino
Journal of the American Chemical Society, 1957 , vol. 79, p. 4427,4429
参考文献
Carpino,L.A.
Journal of the American Chemical Society, 1960 , vol. 82, p. 2725 - 2727
反应条件
1: 0.86 g / DMAP / acetonitrile / 3 h / 20 °C
2: 2.80 g / DMAP / acetonitrile / 2 h / 60 °C
3: 90 percent / Mg(ClO4)2 / acetonitrile / 0.83 h / 50 °C
View Scheme
参考文献
Loog; Maeorg; Ragnarsson
Synthesis, 2000 , # 11 p. 1591 - 1597
参考文献
Pozdnev,V.F.
Zhurnal Organicheskoi Khimii, 1977 , vol. 13, # 12 p. 2531 - 2535,2352 - 2355
反应条件
1.1: pyridine; N-bromosuccinmide / dichloromethane / 0.5 h / 0 °C / Inert atmosphere
2.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -20 °C / Inert atmosphere
2.2: -78 °C / Inert atmosphere
3.1: trifluoroacetic acid / dichloromethane / 0 °C / Inert atmosphere
4.1: [Ru(bpyrz)3](PF6)2*2H2O / methanol; acetonitrile / 24 h / 20 °C / Air; Visible light; Irradiation
View Scheme
参考文献
Zhu, Mingzhao; Zheng, Nan
Synthesis, 2011 , # 14 art. no. C01611SS, p. 2223 - 2236
反应条件
manganese(IV) oxide in dichloromethane
T=20°C; 0.5 h;
参考文献
Kisseljova, Ksenija; Tsubrik, Olga; Sillard, Rannar; Maeeorg, Sirje; Maeeorg, Uno
Organic Letters, 2006 , vol. 8, # 1 p. 43 - 45
反应条件
1: With triethylamine in dichloromethane
2: With trifluoroacetic acid in dichloromethane
T=0°C; 0.5 h;
3: With sodium hydroxide
T=0°C;
参考文献
Chen, Shoujun; Sun, Lijun; Koya, Keizo; Tatsuta, Noriaki; Xia, Zhiqiang; Korbut, Timothy; Du, Zhenjian; Wu, Jim; Liang, Guiqing; Jiang, Jun; Ono, Mitsunori; Zhou, Dan; Sonderfan, Andrew
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 18 p. 5070 - 5076
