1.1: 95 percent / CuI; PdCl2(PPh3)2 / tetrahydrofuran / 18 h / 20 °C
2.1: Bu4NF / tetrahydrofuran / 1.75 h / 0 - 20 °C
3.1: n-BuLi / hexane / -78 - -66 °C
3.2: 36.5 g / diethyl ether; hexane / 1 h / -78 - 20 °C
View Scheme
参考文献
Stevens, Kirk L.; Jung, David K.; Alberti, Michael J.; Badiang, Jennifer G.; Peckham, Gregory E.; Veal, Jim M.; Cheung, Mui; Harris, Philip A.; Chamberlain, Stanley D.; Peel, Michael R.
Organic Letters, 2005 , vol. 7, # 21 p. 4753 - 4756
1.1: Bu4NF / tetrahydrofuran / 1.75 h / 0 - 20 °C
2.1: n-BuLi / hexane / -78 - -66 °C
2.2: 36.5 g / diethyl ether; hexane / 1 h / -78 - 20 °C
View Scheme
参考文献
Stevens, Kirk L.; Jung, David K.; Alberti, Michael J.; Badiang, Jennifer G.; Peckham, Gregory E.; Veal, Jim M.; Cheung, Mui; Harris, Philip A.; Chamberlain, Stanley D.; Peel, Michael R.
Organic Letters, 2005 , vol. 7, # 21 p. 4753 - 4756
