(3-三甲基硅基-2-丙炔基)三苯基溴化磷合成路线 （共 4 条）
反应条件
in o-xylene T=0 - 25°C; Inert atmosphere;
参考文献
Zuercher, Martina; Hof, Fraser; Barandun, Luzi; Schuetz, Andri; Schweizer, W. Bernd; Meyer, Solange; Bur, Daniel; Diederich, Francois
European Journal of Organic Chemistry, 2009 , # 11 p. 1707 - 1719
反应条件
1: 30 percent / Br2, triphenylphosphine / dimethylformamide / 18 h / Ambient temperature 2: 70 percent / benzene / 18 h / Ambient temperature View Scheme
参考文献
Corey,E.J. et al.
Tetrahedron Letters, 1973 , p. 3964 - 3966
参考文献
Eiter,K. et al.
Justus Liebigs Annalen der Chemie, 1978 , p. 658 - 674
反应条件
n-butyllithium in tetrahydrofuran; hexane
T=-78 - -40°C; Inert atmosphere;
参考文献
Sabot, Cyrille; Berard, Didier; Canesi, Sylvain
Organic Letters, 2008 , vol. 10, # 20 p. 4629 - 4632
