1,2-[双-(4-三氟甲基)苯基]乙烷合成路线 （共 12 条）
反应条件
{2,6-(Ph2PO)2-C6H3}NiCl; zinc in N,N-dimethyl-formamide
T=115°C; 16 h; Inert atmosphere;
参考文献
Chen, Tao; Yang, Limin; Li, Liang; Huang, Kuo-Wei
Tetrahedron, 2012 , vol. 68, # 31 p. 6152 - 6157
反应条件
iodine; hypophosphorous acid in acetic acid
24 h; Heating;
参考文献
Fry, Albert J.; Allukian, Myron; Williams, Allison D.
Tetrahedron, 2002 , vol. 58, # 22 p. 4411 - 4415
反应条件
1: pyridine / benzene / Ambient temperature
2: methanol / Irradiation
View Scheme
参考文献
Hilborn; MacKnight; Pincock; Wedge
Journal of the American Chemical Society, 1994 , vol. 116, # 8 p. 3337 - 3346
反应条件
1: (i) EtMgBr, (ii) /BRN= 605365/, (iii) aq. H2SO4
2: (i) nBuLi, (ii) /BRN= 1101680/, (iii) H2, AcOH, PdO
View Scheme
参考文献
Novotny; Collins; Starks
Journal of pharmaceutical sciences, 1973 , vol. 62, # 6 p. 910 - 913
反应条件
2: (i) nBuLi, (ii) /BRN= 1101680/, (iii) H2, AcOH, PdO
View Scheme
参考文献
Novotny; Collins; Starks
Journal of pharmaceutical sciences, 1973 , vol. 62, # 6 p. 910 - 913
反应条件
(i) nBuLi, (ii) /BRN= 1101680/, (iii) H2, AcOH, PdO; Multistep reaction;
参考文献
Novotny; Collins; Starks
Journal of pharmaceutical sciences, 1973 , vol. 62, # 6 p. 910 - 913
反应条件
in acetonitrile
T=24°C; Photolysis; Kinetics; Further Variations:Solvents;
参考文献
Zhang, Xiangyang; Nau, Werner M.
Journal of Physical Organic Chemistry, 2000 , vol. 13, # 10 p. 634 - 639
反应条件
in cyclohexane
Irradiationvarious sulfides; Quantum yieldMechanismProduct distribution;
参考文献
Fleming, Steven A.; Jensen, Anton W.
Journal of Organic Chemistry, 1996 , vol. 61, # 20 p. 7040 - 7044
反应条件
Irradiation; Quantum yield;
参考文献
Givens, Richard S.; Matuszewski, Bogdan; Athey, Phillip S.; Robert Stoner
Journal of the American Chemical Society, 1990 , vol. 112, # 16 p. 6016 - 6021
反应条件
acetone
Irradiation300 nm; Quantum yield;
参考文献
Cristol, Stanley J.; Bindel, Thomas H.
Journal of Organic Chemistry, 1980 , vol. 45, # 6 p. 951 - 957
